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2-Methyl-N-Phenylbenzamide

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Name

2-Methyl-N-Phenylbenzamide

EINECS N/A
CAS No. 7055-03-0 Density 1.144g/cm3
PSA 29.10000 LogP 3.32030
Solubility N/A Melting Point N/A
Formula C14H13NO Boiling Point 276.3oC at 760 mmHg
Molecular Weight 211.263 Flash Point 162.2oC
Transport Information N/A Appearance N/A
Safety Poison by intraperitoneal route. Mildly toxic by ingestion. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx. See also AMIDES. Risk Codes N/A
Molecular Structure Molecular Structure of 7055-03-0 (2-METHYLBENZANILIDE) Hazard Symbols N/A
Synonyms

O-METHYL BENZANILIDE;O-TOLUANILIDE;2-methylbenzoanilide;2-methylbenzoicacidanilide;2-methyl-n-phenyl-benzamid;2-methyl-n-phenylbenzamide;bas305;bas-3050

Article Data 88

2-Methyl-N-Phenylbenzamide Chemical Properties

Chemistry informtion about 2-Methyl-N-Phenylbenzamide (CAS NO.7055-03-0) is:
IUPAC Name: 2-Methyl-N-Phenylbenzamide
Synonyms: O-Methyl Benzanilide ; O-Toluanilide ; 2-Methylbenzoanilide ; 2-Methylbenzoicacidanilide ; 2-Methyl-N-Phenyl-Benzamid ; 2-Methyl-N-Phenylbenzamide ; Bas305 ; Bas-3050
Product Categories: Aromatic Carboxylic Acids , Amides , Anilides , Anhydrides & Salts
MF: C14H13NO
MW: 211.26
EINECS: 230-334-4 
Density: 1.144 g/cm3
Flash Point: 162.2 °C
Boiling Point: 276.3 °C at 760 mmHg
Vapour Pressure: 0.00483 mmHg at 25°C 
Enthalpy of Vaporization: 51.48 kJ/mol
Following is the molecular structure of 2-Methyl-N-Phenylbenzamide (CAS NO.7055-03-0) is:

2-Methyl-N-Phenylbenzamide Uses

2-Methyl-N-Phenylbenzamide (CAS NO.7055-03-0) was used as microbicides, right Einght Control is efficient, particularly for wheat, grains, peanuts, wheat, potato Blight, wheat and root rot sclerotia sexual Rhizoctonia root cause of other diseases have good control. It can also be used to control cotton seedling damping - off, cotton boll rot disease, peanut leaf blight, beet leaf spot, rice blast, such as sheath blight. Rotary medicine, the variety of goods to a certain crop lodging resistance role. Early goods to the application, the application disease Maximum less effective.

2-Methyl-N-Phenylbenzamide Production

Raw materials are Thionyl chloride --> Phosphorus trichloride --> Benzoic acid --> Sodium benzoate --> o-Toluic acid --> o-Toluoyl chloride .

2-Methyl-N-Phenylbenzamide Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intraperitoneal 200mg/kg (200mg/kg)   "Wirksubstanzen der Pflanzenschutz und Schadlingsbekampfungsmittel," Perkow, W., Berlin, Verlag Paul Parey, 1971-1976Vol. -, Pg. -, 1971/1976.
rat LD50 oral 6gm/kg (6000mg/kg)   "Pesticide Index," Frear, E.H., ed., State College, PA, College Science Pub., 1969Vol. 5, Pg. 144, 1976.

2-Methyl-N-Phenylbenzamide Safety Profile

Poison by intraperitoneal route. Mildly toxic by ingestion. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx. See also AMIDES.

2-Methyl-N-Phenylbenzamide Analytical Methods

O-Benzoic acid and phosphorus trichloride for chloride generated reaction intermediates o-benzoyl chloride, with condensation of aniline system in neighboring amide. 24.4kg of aniline, 62.5kg sodium hydroxide solution (100% discount, according to the molar ratio of aniline 1.7 times), 100 kg of toluene were joined enamelled 11:50. Under the mixing temperature 71/92 o-benzoyl chloride, about half an hour increase End 53.0kg. Exothermic reaction, the temperature increase, when about around 70-80 ° C and then heated to 80-90 ° C 30min. After completion of the reaction, to insulation, to join the 90-95 ° C 200L hot water, stirring washed 20min, the formation of sodium chloride and unreacted raw material soluble in water, sewage Still separation of classes. Then water 50-80L, steam distillation, solvent recovery, toluene and trace aniline. Then cold to 30-40 ° C, stirring slowly crystallized into small particles of yellow, filtering, washing coffin-80 ° C dry, in the content of 93-98% of the o-lactamase and the yield more than 95%. The consumption of raw materials fixed : o-benzoic acid (>=80%) 1310kg / t, phosphorus trichloride (>=95%) 740kg / t, aniline (97%) 490kg / t, sodium hydroxide (100%) 1250kg / t.

2-Methyl-N-Phenylbenzamide Specification

2-Methyl-N-Phenylbenzamide (CAS NO.7055-03-0) is a colorless crystalline solid. It can soluble in acetone, dimethyl formamide and dimethyl sulfoxide, methanol, ethanol and majority of organic solvents but insoluble in water. React stablity with acid, alkali and thermal.

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