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2363-59-9

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STEROID HOMOLOG CONTAINING A PYRAZOLE NUCLEUS.
-
VIDA,GUT
p. 792 - 793
(1963)
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Use of [1,2-3H] Testosterone in 5- Reductase Enzymatic Activity Dosing in Dermal Fibroblast Cultures from Polycystic Ovarian Patients
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Matei, L.,Postolache, C.,Fugaru, V.,Condac, E.,Dinichiotu, A.,Costache, M.
p. 1055 - 1056
(2007/10/03)

2-iodo-3-keto-Δ4 steroids, process for their production, as well as their further processing
The new intermediate products of general formula I STR1 in which R1 stands for a hydrogen atom or a straight-chain or branched alkyl group with 1 to 4 carbon atoms, R2 stands for a hydrogen atom or a methyl group, R3 stands for a hydrogen atom, R4 stands for an acyloxy group with 1 to 4 carbon atoms in the acyl radical or R3 and R4 together stand for a keto-oxygen atom, are suitable in an excellent way for introducing a Δ1 double bond in the steroid skelton with the simultaneous presence of a Δ4 double bond, as well as a saturated carbonyl group, by clevage of hydrogen iodide with a base in an amidic solvent at elevated temperature. If R2 stands for a hydrogen atom, the A-ring is aromatized after the hydrogen iodide cleavage. For the production of a new intermediate products, special iodization processes, which partially also allow a stereoselective control of the iodization, are used.
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(2008/06/13)

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Chemical Properties

Melting Point: 149-151 °C
Boiling Point: 443.6 °C at 760 mmHg
Flash Point:192.7 °C
Density: 1.13 g/cm³
Vapor Pressure: 4.58E-08mmHg at 25°C
Refractive Index: 1.555
PSA: 43.37000
LogP: 4.22600

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