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2363-59-9

Basic Information
CAS No.: 2363-59-9
Name: Androsta-1,4-dien-3-one,17-(acetyloxy)-, (17beta)-
Molecular Structure:
Molecular Structure of 2363-59-9 (Androsta-1,4-dien-3-one,17-(acetyloxy)-, (17beta)-)
Formula: C21H28O3
Molecular Weight: 328.44
Synonyms: Androsta-1,4-dien-3-one,17b-hydroxy-, acetate (6CI,7CI,8CI);1,2-Didehydrotestosterone 17-O-acetate;1-Dehydrotestosterone acetate;17beta-Acetoxyandrosta-1,4-dien-3-one;
EINECS: 219-112-8
Density: 1.13 g/cm3
Melting Point: 149-151 °C
Boiling Point: 443.6 °C at 760 mmHg
Flash Point: 192.7 °C
Solubility:
Appearance:
Hazard Symbols: HarmfulXn
Risk Codes: 40-48
Safety: 22-24/25
Transport Information:
PSA: 43.37000
LogP: 4.22600
Synthetic route
108-75-8

2,4,6-trimethyl-pyridine

82926-51-0

17β-acetoxy-2β,4β-dibromo-5β-androstan-3-one

A

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

B

111687-29-7

17β-acetoxy-2-bromo-5β-androst-1-en-3-one

82926-51-0

17β-acetoxy-2β,4β-dibromo-5β-androstan-3-one

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

Conditions
ConditionsYield
With lithium carbonate; lithium bromide
82926-51-0

17β-acetoxy-2β,4β-dibromo-5β-androstan-3-one

A

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

B

111687-29-7

17β-acetoxy-2-bromo-5β-androst-1-en-3-one

Conditions
ConditionsYield
With 2,4,6-trimethyl-pyridine
15359-18-9

17β-Acetoxy-3-oxo-Δ1,5-androstadien

108-24-7

acetic anhydride

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

Conditions
ConditionsYield
(i) (UV-irradiation), EtOH, (ii) KOH, MeOH, (iii) /BRN= 385737/, Py; Multistep reaction;
1045-69-8

testosterone acetate

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

Conditions
ConditionsYield
With thallium(III) acetate In acetic acid
With 2,6-dichloro-3,5-dicyano-1,4-benzoquinone
2α.4α-dibromo-17β-acetoxy-androstanone-(3)

2α.4α-dibromo-17β-acetoxy-androstanone-(3)

A

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

B

17β-acetoxy-androstadien-(4.6)-one-(3)

17β-acetoxy-androstadien-(4.6)-one-(3)

Conditions
ConditionsYield
With 2,3,5-trimethyl-pyridine
82926-51-0

17β-acetoxy-2β,4β-dibromo-5β-androstan-3-one

68-12-2, 33513-42-7

N,N-dimethyl-formamide

LiBr

LiBr

Li2CO3

Li2CO3

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

Conditions
ConditionsYield
60 min;
58-22-0

testosterone

<2,4,6-triiodo-phenoxy>-acetyl chloride

<2,4,6-triiodo-phenoxy>-acetyl chloride

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 2,6-dichloro-3,5-dicyano-1,4-benzoquinone
View Scheme
1164-92-7

17β-acetoxy-5β-androstan-3-one

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: acetic acid; bromine
2: 2,4,6-trimethyl-pyridine
View Scheme

Acetic acid (8R,9S,10R,13S,14S,17S)-6-bromo-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-17-yl ester

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Zn / aq. ethanol
2: (i) (UV-irradiation), EtOH, (ii) KOH, MeOH, (iii) /BRN= 385737/, Py
View Scheme
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

75-24-1

trimethylaluminum

5824-29-3

17β-acetyloxy-1α-methylandrost-4-en-3-one

Conditions
ConditionsYield
copper(I) bromide In 1,4-dioxane; water; toluene75.58%
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

84871-43-2

17β-acetoxyandrosta-1,4-diene-3-thione

Conditions
ConditionsYield
With Lawessons reagent In tetrahydrofuran for 1h; Ambient temperature;60%
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

1045-69-8

testosterone acetate

Conditions
ConditionsYield
With thallium(III) nitrate trihydrate In diethylene glycol dimethyl ether for 24h; Ambient temperature;34%
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

97455-04-4

androsta-1,4-diene-11α,17β-diol-3-one, 17-acetate

Conditions
ConditionsYield
for 72h; Rhizopus arrhizus ATCC 11145;15%
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

6223-90-1

17β-acetoxy-2-methyl-estra-1,3,5(10)-trien-4-ol

Conditions
ConditionsYield
With 1,4-dioxane Irradiation.UV-Licht;
In 1,4-dioxane for 9h; Irradiation;
In methanol Heating; Irradiation;
Multi-step reaction with 2 steps
1: dioxane / Irradiation
2: dioxane / Irradiation
View Scheme
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

1855-85-2

17β-acetoxy-2-hydroxy-4-methyl-19-norpregna-1,3,5(10)-triene

Conditions
ConditionsYield
With 1,4-dioxane Irradiation.UV-Licht;
In 1,4-dioxane for 9h; Irradiation;
With acetic acid Heating; Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

2242-09-3

17β-acetoxy-1-hydroxy-4-methylestra-1,3,5(10)-triene

Conditions
ConditionsYield
With 1,4-dioxane Irradiation.UV-Licht;
In 1,4-dioxane for 9h; Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

2456-11-3

17β-acetoxy-1-methyl-estra-1,3,5(10)-trien-3-ol

Conditions
ConditionsYield
With 1,4-dioxane Irradiation.UV-Licht;
In 1,4-dioxane for 9h; Irradiation;
In methanol Heating; Irradiation;
Multi-step reaction with 2 steps
1: dioxane / Irradiation
2: dioxane / Irradiation
View Scheme
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

A

2383-80-4, 2587-20-4

(1Ξ,6Ξ,3'aS)-6't-acetoxy-4,5'a-dimethyl-(3'ar,5'at,8'ac,8'bt)-decahydro-spiro[bicyclo[3.1.0]hex-3-ene-6,3'-As-indacen]-2-one

B

2363-60-2, 2506-73-2, 114029-64-0

17β-acetoxy-1β,5β-cyclo-10α-androst-3-en-2-one

Conditions
ConditionsYield
With 1,4-dioxane Irradiation.UV-Licht;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

A

14407-07-9, 14532-16-2

(1Ξ,3'aS)-6't-acetoxy-4,5'a-dimethyl-(3'ar,5'at,8'ac,8'bt)-decahydro-spiro[cyclohexa-3,5-diene-1,3'-As-indacen]-2-one

B

2456-09-9, 6173-73-5

(1Ξ,3'aS)-6't-acetoxy-2,5'a-dimethyl-(3'ar,5'at,8'ac,8'bt)-decahydro-spiro[cyclohexa-2,5-diene-1,3'-As-indacen]-4-one

Conditions
ConditionsYield
With 1,4-dioxane Irradiation.UV-Licht;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

41982-55-2, 95118-63-1

17β-acetoxy-6β-bromo-androsta-1,4-dien-3-one

Conditions
ConditionsYield
With N-Bromosuccinimide; dibenzoyl peroxide
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

2383-80-4, 2587-20-4

(1Ξ,6Ξ,3'aS)-6't-acetoxy-4,5'a-dimethyl-(3'ar,5'at,8'ac,8'bt)-decahydro-spiro[bicyclo[3.1.0]hex-3-ene-6,3'-As-indacen]-2-one

Conditions
ConditionsYield
In 1,4-dioxane for 1.5h; Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

2363-60-2

2-Oxo-17β-acetoxy-1α.5β-cyclo-Δ3-10α-androsten

Conditions
ConditionsYield
In 1,4-dioxane for 1.5h; Irradiation;
With acetic acid Heating; Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

14407-07-9, 14532-16-2

(1Ξ,3'aS)-6't-acetoxy-4,5'a-dimethyl-(3'ar,5'at,8'ac,8'bt)-decahydro-spiro[cyclohexa-3,5-diene-1,3'-As-indacen]-2-one

Conditions
ConditionsYield
In 1,4-dioxane for 1.5h; Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

2456-09-9, 6173-73-5

(1Ξ,3'aS)-6't-acetoxy-2,5'a-dimethyl-(3'ar,5'at,8'ac,8'bt)-decahydro-spiro[cyclohexa-2,5-diene-1,3'-As-indacen]-4-one

Conditions
ConditionsYield
In 1,4-dioxane for 1.5h; Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

108-24-7

acetic anhydride

798-35-6

17β-acetoxy-4-methylestra-1,3,5(10)-triene

Conditions
ConditionsYield
(i) LiAlH4, Et2O, (ii) /BRN= 385737/, Py; Multistep reaction;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

122-52-1

triethyl phosphite

14413-08-2

1-Diaethoxyphosphinyl-testosteron-acetat

Conditions
ConditionsYield
With phenol
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

A

977-83-3

17β-acetoxy-2-chloroandrosta-1,4-diene-3-one

B

62799-78-4

17β-acetoxy-4-chloroandrosta-1,4-diene-3-one

Conditions
ConditionsYield
With pyridine; sulfuryl dichloride for 1h; Ambient temperature;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

17β-acetoxy-4ξ,5ξ-dihydroxy-1-androsten-3-one

17β-acetoxy-1ξ,2ξ-dihydroxy-4-androsten-3-one

Conditions
ConditionsYield
With osmium(VIII) oxide; potassium chlorate In water; tert-butyl alcohol for 600h; Ambient temperature; Yield given. Yields of byproduct given;
593-77-1

N-Methylhydroxylamine

2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

A

84871-34-1, 84871-35-2

(Z)-17β-acetoxy-3-methylimino-1,4-androstadiene N-oxide

B

84871-34-1, 84871-35-2

(E)-17β-acetoxy-3-methylimino-1,4-androstadiene N-oxide

Conditions
ConditionsYield
With pyridine at 40℃; Yield given. Yields of byproduct given;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

3-Oxo-17β-acetoxy-Δ1:10.19-1(10->5)-abeo-5α-androstadien

Conditions
ConditionsYield
With acetic acid Heating; Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

73398-07-9

3-Oxo-10β-hydroxy-17β-acetoxy-Δ1-1(10->5)-abeo-5α-androsten

Conditions
ConditionsYield
With acetic acid Heating; Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

15267-01-3

3β,5aβ-Dimethyl-6β-acetoxy-(3aα,8aα,8bβ)-perhydro-cyclopent-inden-3α-carbonsaeure

Conditions
ConditionsYield
(i) O3, AcOEt, (ii) aq. H2O2; Multistep reaction;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

3-Oxo-17β-acetoxy-Δ1.9-1(10->5)-abeo-5α-androstadien

Conditions
ConditionsYield
With acetic acid Heating; Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

2242-10-6

1-Oxo-4α-methyl-17β-acetoxy-4β.10β-cyclo-(9(10-5β)-abeo-Δ2-10αH-oestren

Conditions
ConditionsYield
In 1,4-dioxane Irradiation;
2363-59-9

17β-acetoxy-androsta-1,4-dien-3-one

1-Oxo-3-methyl-17β-acetoxy-4α.10α-cyclo-(9(10-5β)-abeo-Δ2-10βH-oestren

Conditions
ConditionsYield
In 1,4-dioxane Irradiation;
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  • 2363-59-9   Androsta-1,4-dien-3-one,17-(acetyloxy)-, (17beta)-

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    2363-59-9 Androsta-1,4-dien-3-one,17-(acetyloxy)-, (17beta)-

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    Boldenone 17-acetate cas 2363-59-9

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Specification

The Boldenone 17-acetate, with the CAS registry number 2363-59-9, is also known as (17beta)-Hydroxyandrosta-1,4-dien-3-one acetate. It belongs to the product category of Steroids. Its EINECS registry number is 219-112-8. This chemical's molecular formula is C21H28O3 and molecular weight is 328.45. Its IUPAC name is called [(8R,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-6,7,8,9,11,12,14,15,16,17-decahydrocyclopenta[a]phenanthren-17-yl] acetate.

Physical properties of Boldenone 17-acetate: (1)ACD/LogP: 4.39; (2)ACD/LogD (pH 5.5): 4.39; (3)ACD/LogD (pH 7.4): 4.39; (4)ACD/BCF (pH 5.5): 1286.17; (5)ACD/BCF (pH 7.4): 1286.17; (6)ACD/KOC (pH 5.5): 5851.06; (7)ACD/KOC (pH 7.4): 5851.06; (8)#H bond acceptors: 3; (9)#Freely Rotating Bonds: 2; (10)Index of Refraction: 1.555; (11)Molar Refractivity: 92.6 cm3; (12)Molar Volume: 288.3 cm3; (13)Surface Tension: 43.3 dyne/cm; (14)Density: 1.13 g/cm3; (15)Flash Point: 192.7 °C; (16)Enthalpy of Vaporization: 70.13 kJ/mol; (17)Boiling Point: 443.6 °C at 760 mmHg; (18)Vapour Pressure: 4.58E-08 mmHg at 25°C.

When you are using this chemical, please be cautious about it. This chemical may cause damage to health. There will be a danger of serious damage to health by prolonged exposure. In addition, you should not breathe its dust. Finally, you must avoid contact with skin and eyes.

You can still convert the following datas into molecular structure:
(1)SMILES: O=C\1\C=C/C4(/C(=C/1)CCC3C4CCC2(C3CCC2OC(=O)C)C)C
(2)InChI: InChI=1/C21H28O3/c1-13(22)24-19-7-6-17-16-5-4-14-12-15(23)8-10-20(14,2)18(16)9-11-21(17,19)3/h8,10,12,16-19H,4-7,9,11H2,1-3H3
(3)InChIKey: KPCDGGNHYODURF-UHFFFAOYAO