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58-19-5

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Cyclopropanation of steroidal A-ring 2-enol derivatives
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Templeton,Paslat,Wie
p. 2058 - 2064
(1978)
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NEUROACTIVE STEROIDS, COMPOSITIONS, AND USES THEREOF
Described herein are neuroactive steroids of the Formula (I): (Formula (I)) or a pharmaceutically acceptable salt thereof; wherein R1a and R1b are as defined herein. Such compounds are envisioned, in certain embodiments, to behave as GABA modulators. The present invention also provides pharmaceutical compositions comprising a compound of the present invention and methods of use and treatment, e.g., such for inducing sedation and/or anesthesia.
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Paragraph 112

(2015/02/02)

Synthesis of 2α-methyldihydrotestosterone from tigogenin
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Sikharulidze,Merlani,Amiranashvili
p. 294 - 294
(2007/10/03)

Ring A Conformation in Steroids 2 -NMR Study of C-2 Monomethyl- and Dimethyl-Substituted 5α-Androstan-3-ones
Ring A proton shifts and couplings and 13C shifts of all carbons are given for 17β-acetoxy-2α-methyl- and 17β-methoxy-2β-methyl-5α-androstan-3-one and 2,2-dimethyl-17β-methoxy-5α-androstan-3-one.It was concluded that the 2α-methyl derivative exists with ring A in a regular chair conformation while the 2β-methyl derivative exists with ring A in an inverted boat conformation with C-2 and C-5 at the bow/stern positions.The data for 2,2-dimethyl-17Β-methoxy-5α-androstan-3-one suggest an equilibrium of these two conformers.KEY WORDS 1H NMR 13C NMR monomethyl/dimethyl 5α-androstan-3-ones Steroid Ring A conformation
Marat, Kirk,Templeton, John F.,Gupta, R. K.,Kumar, Sashi V. P.
p. 730 - 733
(2007/10/02)

STEROIDS. CCIX. RING A MODIFIED HORMONE ANALOGS. V.
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EDWARDS,CALZADA,BOWERS
p. 178 - 182
(2007/10/10)

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Chemical Properties

Melting Point: 149-153oC
Boiling Point: 420.3°Cat760mmHg
Flash Point:179.4°C
Density: 1.058g/cm³
Storage Temp.:Refrigerator
Vapor Pressure: 7.98E-09mmHg at 25°C
PKA: 15.09±0.70(Predicted)
PSA: 37.30000
LogP: 4.20510

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