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Conditions | Yield |
---|---|
With diiron nonacarbonyl In benzene at 40 - 50℃; for 2.5h; | 90% |
With triiron dodecarbonyl at 25 - 30℃; for 1h; Irradiation; | 85% |
With potassium tert-butylate In dimethyl sulfoxide at 70℃; for 0.833333h; Inert atmosphere; | 70% |
(PMe3)2Rh(D2O)2*BF4 In water-d2 at 25℃; for 0.5h; | 95 % Spectr. |
Conditions | Yield |
---|---|
2-ethyl-N-(2-ethylhexyl)-1-hexanamine; toluene-4-sulfonic acid | 77.5% |
With quinoline; phosphorus pentoxide distillation at a bath temp. 150 deg C; | 75% |
With quinoline; phosphorus pentoxide vermutlich entsteht als Gemisch von cis- und trans-Form; | |
With sodium hydrogen sulfate vermutlich entsteht als Gemisch von cis- und trans-Form; | |
With silver-asbestos at 280℃; vermutlich entsteht als Gemisch von cis- und trans-Form; |
3-ethoxy-2-methyl-acrylic acid
A
ethyl 1-propenyl ether
B
methylammonium carbonate
ethyl 1-propenyl ether
Conditions | Yield |
---|---|
bei vorsichtigem Kochen; |
Conditions | Yield |
---|---|
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride In benzene-d6 at 60℃; for 1h; |
3-ethoxyprop-1-ene
Triethoxysilane
A
ethylpropylether
B
ethyl 1-propenyl ether
C
triethoxy(3-ethoxypropyl)silane
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex In 5,5-dimethyl-1,3-cyclohexadiene; diethylene glycol dimethyl ether at 70℃; for 12h; Inert atmosphere; |
3-ethoxyprop-1-ene
tris(2-methoxyethoxy)silane
A
ethylpropylether
B
ethyl 1-propenyl ether
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex In 5,5-dimethyl-1,3-cyclohexadiene; toluene at 70℃; for 12h; Inert atmosphere; |
Conditions | Yield |
---|---|
In benzene at 80℃; for 24h; | 100% |
5-iodo-6-methyl-N-[4-(methylsulfonyl)benzyl]-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxamide
ethyl 1-propenyl ether
Conditions | Yield |
---|---|
Stage #1: 5-iodo-6-methyl-N-[4-(methylsulfonyl)benzyl]-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxamide; ethyl 1-propenyl ether With triethylamine; bis[1,2-bis(diphenylphosphino)ethane]palladium(0) In DMF (N,N-dimethyl-formamide) at 100℃; Stage #2: With hydrogenchloride; water In DMF (N,N-dimethyl-formamide) for 1.5h; | 99% |
Stage #1: 5-iodo-6-methyl-N-[4-(methylsulfonyl)benzyl]-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxamide; ethyl 1-propenyl ether With triethylamine; bis[1,2-bis(diphenylphosphino)ethane]palladium(0) In DMF (N,N-dimethyl-formamide) at 100℃; Stage #2: With hydrogenchloride; water In DMF (N,N-dimethyl-formamide) for 1.5h; | 99% |
ethyl 1-propenyl ether
diphenyl ketene
3-ethoxy-4-methyl-2,2-diphenylcyclobutanone
Conditions | Yield |
---|---|
In diethyl ether at 20℃; | 99% |
Molecular structure of Ether, ethyl propenyl (CAS NO.928-55-2) is:
Product Name: Ether, ethyl propenyl
CAS Registry Number: 928-55-2
IUPAC Name: (Z)-1-ethoxyprop-1-ene
Molecular Weight: 86.1323 [g/mol]
Molecular Formula: C5H10O
XLogP3-AA: 1.4
H-Bond Donor: 0
H-Bond Acceptor: 1
EINECS: 213-176-0
Refractive index: n20/D 1.398(lit.)
Storage temp.: Flammables area
Water Solubility: soluble
Surface Tension: 21 dyne/cm
Density: 0.775 g/cm3
Flash Point: -2 °F
Enthalpy of Vaporization: 29.71 kJ/mol
Boiling Point: 68.2 °C at 760 mmHg
Vapour Pressure: 153 mmHg at 25°C
Classification Code: Skin / Eye Irritant
Ether, ethyl propenyl (CAS NO.928-55-2) is used in organic synthesis.It is also used in coating, adhesive, additives, plasticizer, etc.
Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
---|---|---|---|---|---|
rabbit | LD50 | skin | 3970uL/kg (3.97mL/kg) | Toxicology and Applied Pharmacology. Vol. 28, Pg. 313, 1974. | |
rat | LCLo | inhalation | 8000ppm/4H (8000ppm) | Toxicology and Applied Pharmacology. Vol. 28, Pg. 313, 1974. | |
rat | LD50 | oral | 4660uL/kg (4.66mL/kg) | Toxicology and Applied Pharmacology. Vol. 28, Pg. 313, 1974. |
Hazard Codes: F, Xi
Risk Statements: 11-36/37/38
R11:Highly flammable.
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 16-26-36/37/39-37/39
S16:Keep away from sources of ignition.
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
S37/39:Wear suitable gloves and eye/face protection.
RIDADR: UN 3271 3/PG 2
WGK Germany: 3
RTECS: KO0525000
HazardClass: 3
PackingGroup: II
Ether, ethyl propenyl , its cas register number is 928-55-2. It also can be called 1-Ethoxy-1-propene ; 1-Ethoxypropene ; Ethyl 1-propenyl ether ; Ethyl propenyl ether ; Propenyl ethyl ether ; 1-Propene, 1-ethoxy- .It is a clear colorless to light yellow liquid.