Journal of Organic Chemistry p. 336 - 338 (1987)
Update date:2022-09-26
Topics:
Marx, John N.
Bih, Qoang-Rung
A seven-step total synthesis of 1 is reported, starting with 3,5-dimethylphenol.Formylation with Zn(CN)2 gives 9.Mesylation of the derived alcohol 10 occurs only on the phenolic OH, to give 12.Coupling of this with the dilithium salt 15 of 2,3-dimethylbut
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