8,10-Dimethyl-7,13-dioxa-10-azaspirotridecane - the first representative of perhydro-1,3-dioxa-6-azocines

Article abstract of DOI:10.1007/BF01151310

The first representative of perhydro-1,3-dioxa-6-azocines, 8,10-dimethyl-7,13-dioxa-10-azaspiro<5,7>tridecane, was synthesized by the reaction of 4-methyl-1-oxa-4-azaspiro<4,5>-decane with propylene oxide.The structure of the compound has been confirmed by IR and 1H and 13C NMR spectroscopy and mass spectrometry. - Key words: 8,10-dimethyl-7,13-dioxa-10-azaspiro<5,7>tridecane, perhydro-1,3-dioxa-6-azocines; 4-methyl-1-oxa-4-azaspiro<4,5>-decane, propylene oxide, reaction.