Magnetic Resonance in Chemistry p. 292 - 296 (1986)
Update date:2022-08-03
Topics:
Begley, Michael J.
Crabb, Trevor A.
Roch, Olive G.
2-(Piperidin-2-ylmethyl)cycloalkanols have been synthesized by the reaction between 2-picolyllithium and cycloalkene oxides, followed by catalytic hydrogenation of the resulting 2-(pyridin-2-ylmethyl)cycloalkanols.The configurations of the 2-(piperidin-2-yl-methyl)cycloalkanols were assigned by comparing their 13C and 1H NMR parameters with those of 2-(piperidin-2-ylmethyl)cyclohexanols of known (x-ray) configuration.
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