Novel syntheses of 2,3-dihydro-5H-1,4-benzoxathiepins and 1,2,3,5-tetrahydro-4,1-benzothiazepines

DOI: 10.1002/jhet.5570230439

Source and publish data:

Journal of Heterocyclic Chemistry p. 1163 - 1166 (1986)

Update date:2022-08-05

Topics: Oxidation   Column chromatography   NMR spectroscopy   Catalyst   Nucleophile   Electrophile   Synthetic route   Reduction   Recrystallization   Mass spectrometry (MS)   Cyclization   Reaction Time   Reaction Monitoring   Solvent Selection   Reaction Optimization   Heterocyclic compound   Yield calculation   Stirring rate  

Authors:

Ishibashi

Okada

Akiyama

et al.