
Journal of the Chemical Society. Perkin transactions I p. 1739 - 1742 (1987)
Update date:2022-08-05
Topics:
Maskill, H.
The previously unknown methoxy substituted benzene derivative 2,3,3a,4,5,6-hexahydro-8-methoxy-1H-phenalene (3a) has been prepared by two routes.One starts from 6-methoxy-α-tetralone (4a) and involves a single 3-carbon extension and cycization of the alcohol (7b); the other starts from 3-(3-methoxyphenyl)propanoic acid (5a) and proceeds via a 4-carbon extension and a double cyclization of the diol (10).
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