Synthesis and Structural Analysis of 5-Deoxy-3-O-methyl-5-C--α- and β-D-xylopyranoses

DOI: 10.1246/bcsj.61.2499

Source and publish data:

Bulletin of the Chemical Society of Japan p. 2499 - 2506 (1988)

Update date:2022-07-31

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Authors:

Hanaya, Tadashi

Shigetoh, Nobuyuki

Yamamoto, Hiroshi

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Article abstract of DOI:10.1246/bcsj.61.2499

Treatment of 5-deoxy-5-iodo-1,2-O-isopropylidene-3-O-methyl-α-D-xylofuranose with ethyl phenylphosphinothioate in the presence of NaH in DMF gave a 1:1 mixture of the 5-deoxy-5-C-<(R)- and (S)-(ethoxy)phenylphosphinothioyl> derivatives.Reduction of these

Full text of DOI:10.1246/bcsj.61.2499

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