Journal of Coordination Chemistry p. 296 - 306 (2010)
Update date:2022-07-31
Topics: Catalysts Complexes Thiosemicarbazone chalcone Ruthenium(III)
Muthukumar
Sivakumar
Viswanathamurthi
Karvembu
Prabhakaran
Natarajan
New six-coordinate ruthenium(III) complexes [RuX(EPh3)2(L)] (X = Cl or Br; E = P or As; L = chalcone thiosemicarbazone) have been prepared by reacting [RuX3(EPh3)3] (X = Cl or Br; E = P or As) with chalcone thiosemicarbazones in benzene under reflux. The new complexes have been characterized by analytical and spectroscopic (IR, electronic, mass, and EPR) data. The redox behavior of the complexes has also been studied. Based on the above data, an octahedral structure has been assigned for all the complexes. The new complexes exhibit catalytic activity for carbon-carbon coupling reactions.
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