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500-66-3

Basic Information
CAS No.: 500-66-3
Name: 1,3-Benzenediol,5-pentyl-
Article Data: 44
Cas Database
Molecular Structure:
Molecular Structure of 500-66-3 (1,3-Benzenediol,5-pentyl-)
Formula: C11H16O2
Molecular Weight: 180.247
Synonyms: 5-Pentylbenzene-1,3-diol;1,3-Dihydroxy-5-pentylbenzene;3,5-Dihydroxyamylbenzene;Resorcinol, 5-pentyl- (8CI);Olivetol(6CI);5-n-Amylresorcinol;5-Pentylresorcinol;5-n-Pentylresorcinol;
EINECS: 207-908-8
Density: 1.069 g/cm3
Melting Point: 46-48 °C(lit.)
Boiling Point: 313.259 °C at 760 mmHg
Flash Point: 148.758 °C
Solubility: insoluble in water
Appearance: light purple to brown crystalline mass
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/39
Transport Information: N/A
PSA: 40.46000
LogP: 2.83050
Synthetic route
22976-40-5

1,3-dimethoxy-5-pentylbenzene

500-66-3

Olivetol

Conditions
ConditionsYield
With boron tribromide In dichloromethane at -15 - 20℃; for 1.5h; Solvent; Reagent/catalyst; Inert atmosphere;95%
With boron tribromide In dichloromethane at -15 - 20℃; for 1.5h; Inert atmosphere;92%
With boron tribromide In dichloromethane at -15 - 20℃; for 1.5h; Inert atmosphere;92%
58016-28-7

methyl 2,4-dihydroxy-6-pentylbenzoate

500-66-3

Olivetol

Conditions
ConditionsYield
With water; potassium hydroxide at 50 - 100℃;94%

1,3-Bis-benzyloxy-5-((Z)-pent-1-enyl)-benzene

500-66-3

Olivetol

Conditions
ConditionsYield
With sodium; butan-1-ol at 80 - 90℃; for 1h;81%
With hydrogen; palladium on activated charcoal In ethanol Yield given;

3,5-diamino-1-pentylbenzene

500-66-3

Olivetol

Conditions
ConditionsYield
Stage #1: 3,5-diamino-1-pentylbenzene With sulfuric acid; sodium nitrite In dichloromethane at 5℃;
Stage #2: With sulfuric acid; sodium sulfate In water for 1h; Reflux;
78%
27871-89-2

methyl 6-n-pentyl-2-hydroxy-4-oxo-cyclohex-2-ene-1-carboxylate

500-66-3

Olivetol

Conditions
ConditionsYield
With bromine In N,N-dimethyl-formamide at 160℃; for 10h; Cooling with ice;69.3%
With bromine In N,N-dimethyl-formamide at 80 - 160℃;69.3%
With bromine In N,N-dimethyl-formamide at 160℃; for 11.5h; Cooling with ice;69.3%
With bromine In N,N-dimethyl-formamide at 160℃; for 10h; Cooling with ice;69.3%
With bromine In N,N-dimethyl-formamide at 80 - 160℃; for 11.5h; Cooling with ice;69.3%
74732-76-6

4-Benzenesulfinyl-5-pentyl-cyclohexane-1,3-dione

500-66-3

Olivetol

Conditions
ConditionsYield
With calcium carbonate In benzene for 5h; Heating;48%
58016-30-1

5-n-amyl-2-bromocyclohex-2-ene-3-ol-1-one

A

78463-35-1

4-bromo-5-pentylbenzene-1,3-diol

B

78463-34-0

4,6-dibromo-5-pentylbenzene-1,3-diol

C

500-66-3

Olivetol

Conditions
ConditionsYield
In diphenylether heating to 155 deg C during 1 h;A 32%
B 10%
C 40%
67-56-1

methanol

491-47-4

olivetoric acid

A

3734-54-1

6,8-dihydroxy-3-pentyl-1H-2-benzopyran-1-one

B

500-66-3

Olivetol

Conditions
ConditionsYield
at 150 - 200℃;
64-18-6

formic acid

491-47-4

olivetoric acid

A

3734-54-1

6,8-dihydroxy-3-pentyl-1H-2-benzopyran-1-one

B

500-66-3

Olivetol

628-13-7

pyridine hydrochloride

A

99-87-6

4-methylisopropylbenzene

B

500-66-3

Olivetol

Conditions
ConditionsYield
at 210 - 230℃;
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    Name:Olivetol Synonyms:3,5-Dihydroxyamylbenzene; 5-Pentyl-1,3-benzenediol; 5-Pentylresorcinol;Pentyl-3,5-dihydroxybenzene Molecular Formula:C11H16O2 Molecular Weight:180.25 CAS Number:500-66-3 EINECS:207-908-8 Purity:98% Apearance:off-white po

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    Name:Olive alcohol The alias:3, 5-dihydroxypentylene CAS NO:500-66-3 Molecular formula:C11H16O2 Molecular weight:180.24 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage Se

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Chemistry

Molecular Formula: C16H26N2O2
Molecular Weight: 278.3898 g/mol 
EINECS: 207-908-8 
Index of Refraction: 1.546
Surface Tension: 43.5 dyne/cm 
Melting point: 46-48 °C
Density: 1.068 g/cm3
Flash Point: 148.8 °C
Solubility in water: Slightly soluble
Enthalpy of Vaporization: 57.64 kJ/mol
Boiling Point: 313.3 °C at 760 mmHg
Vapour Pressure: 0.000273 mmHg at 25 °C 
Appearance: Off-white crystals or olive to light purple waxy solid
Product Category of Olivetol (CAS NO.500-66-3): API intermediates
Following is the structure of Olivetol (CAS NO.500-66-3): 
    
 

Safety Profile

Hazard Codes:IrritantXi
Risk Statements: 36/37/38 
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/39 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36:Wear suitable protective clothing. 
S39:Wear eye / face protection.
WGK Germany: 3
RTECS: VH2880000

Specification

 Olivetol, its cas register number is 500-66-3. It also can be called  3,5-Dihydroxyamylbenzene ; 3-06-00-04695 (Beilstein Handbook Reference) ; 5-Pentyl-1,3-benzenediol ; 5-Pentylresorcinol ; 5-n-Amylresorcinol ; 5-n-Pentylresorcinol. And its IUPAC name is [3-(diethylamino)-2,2-dimethylpropyl] 4-aminobenzoate. Olivetol (CAS NO.500-66-3) is hazardous, so the first aid measures and others should be known. Such as: When on the skin: first, should flush skin with plenty of water immediately for at least 15 minutes while removing contaminated clothing and shoes. Secondly, get medical aid. Or in the eyes: Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Then get medical aid soon. While, it's inhaled: Remove from exposure and move to fresh air immediately. If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Get medical aid. And as soon as to get medical aid. If you have the ingesting of the product : Never give anything by mouth to an unconscious person. Get medical aid. Do not induce vomiting. If conscious and alert, rinse mouth and drink 2-4 cupfuls of milk or water.
In addition, Olivetol should be stored in a tightly closed container, or stored in a cool, dry, well-ventilated area away from incompatible substances as well as stored protected from light.