Tetrahedron p. 13335 - 13346 (1994)
Update date:2022-08-03
Topics: Column chromatography Stereochemistry Recrystallization Mass spectrometry (MS) Optical rotation HPLC (high-performance liquid chromatography) Protecting group Chiral Resolution Chirality Antiviral agents Enantiospecific synthesis Hydroxymethyl NMR spectroscopy (Nuclear Magnetic Resonance) Synthetic yield
Hosono
Nishiyama
Yamamura
Izawa
Kato
Terada
The enantiospecific synthesis of [(2'S, 3'S)-bis(hydroxymethyl)azatidin-1-yl]pyrimidine nucleotides 22, 25, and 27 was achieved via construction of the base on the 1-aminoacetidine 18 prepared from (+)-diethyl-L-tartrate, and they are the first members of
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