Journal of Organometallic Chemistry p. 289 - 294 (1990)
Update date:2022-08-02
Topics:
Fronda, Antonio
Maas, Gerhard
Reaction of Ph2tBuSiSnMe3 or iPr3SiSnMe3 with triflic acid (CF3SO3H; TfOH) at -40 deg C yields the first silylstannyl triflates, Ph2tBuSiSnMe2OTf and iPr3SiSnMe2OTf.The former triflate is thermally unstable above 0 deg C, but the latter has been isolated as a thermally stable crystalline solid.Both triflates can be used for efficient silylstannylation of ehtyl diazoacetate.
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