Canadian Journal of Chemistry p. 1137 - 1140 (2005)
Update date:2022-08-04
Topics: Characterization Mitsunobu reaction Purification Workup Reaction Setup
Arora, Revika
Paul, Satya
Gupta, Rajive
A mild and efficient procedure has been developed for the conversion of aromatic carboxylic esters to secondary amides using reusable Zn dust with microwave heating in the presence of N,N-dimethylformamide or conventional heating by stirring in an oil bath using THF as solvent. Zn dust can be reused several times after simple washing with dil. HC1 and distilled water.
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