Tetrahedron p. 7471 - 7481 (1990)
Update date:2022-08-04
Topics:
Nakamura, Kaoru
Kitayama, Takashi
Inoue, Yoshihiko
Ohno, Atsuyoshi
The α-position to the nitro group in 4-nitro-2-butanol or 5-nitro-2-pentanol was acylated under DBU-catalysis after the hydroxy group was protected by a t-butyl dimethylsilyl group. The present method has been applied to the asymmetric stereoselective synthesis of a pheromone for Andrena haemorrhoa F, which has an interesting spiroacetal strucure.
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