Bulletin of the Chemical Society of Japan p. 89 - 92 (1986)
Update date:2022-08-04
Topics: Solvent Reagent Temperature Starting Material Work-Up Product Isolation Reaction Procedure
Miyake, Hideyoshi
Yamamura, Kimiaki
The nitro group, activated by a carbonyl group, alkoxycarbonyl group or a phenyl group, can be replaced by a phenylthio group in the reaction with benzenethiol or its potassium salt.This reaction proceeds in the electron transfer mechanism, and is applicable to the general syntheses of α-phenylthio ketones, α-phenylthio carboxylic esters and α-phenylthio alkylbenzenes from primary nitro compounds.
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