Tetrahedron Letters p. 1499 - 1502 (1991)
Update date:2022-08-03
Topics:
Dommerholt
Thijs
Zwanenburg
By means of a total synthesis, the absolute configuration of the naturally occurring macrodiolide pyrenophorol has been established. An essential step is the photo-induced rearrangement of an α,β-epoxy diazomethyl ketone to produce a 4-hydroxy-2-alkenoate. The two lactone units have been introduced in two successive steps.
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