Organic and Biomolecular Chemistry p. 7990 - 7992 (2011)
Update date:2022-08-03
Topics:
Dethe, Dattatraya H.
Ranjan, Alok
Pardeshi, Vijendra H.
Asymmetric first total syntheses of the unprecedented toxins oxazinin-5, oxazinin-6 and preoxazinin-7 have been achieved from a common key intermediate 18, derived from a regiocontrolled Sharpless asymmetric aminohydroxylation and oxa-Michael reaction, which in addition to confirming the structure also established the absolute configuration of the natural products. On the way an expeditious synthesis of a metabolite bursatellin was completed in 8 steps. The Royal Society of Chemistry 2011.
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