Advanced Synthesis and Catalysis p. 1628 - 1633 (2018)
Update date:2022-08-03
Topics:
Nath, Utpal
Chowdhury, Deepan
Pan, Subhas Chandra
The first nonenzymatic DKR reaction of hemithioacetals is developed. Hemithioacetals were formed in situ via thiol addition and subsequently underwent an intramolecular oxa-Michael reaction. The scope of the reaction was quite broad ranging from aliphatic to aromatic substituents and 1,3-disubstituted-1,3-dihyroisobenzofuran products were obtained in good yields with moderate diastereoselectivities and high enantioselectivities. (Figure presented.).
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