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1,3-Diaminopropane 99% CAS:109-76-2 from FandaChem
Cas No: 109-76-2
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1,3-DiaMinopropane CAS NO.109-76-2
Cas No: 109-76-2
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1,3-Diaminopropane Manufacturer/High quality/Best price/In stock
Cas No: 109-76-2
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High quality 1,3-Propane Diamine supplier in China
Cas No: 109-76-2
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1,3-Diaminopropane
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1,3-DiaMinopropane
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Factory Supply Trimethylenediamine
Cas No: 109-76-2
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Amadis Chemical offer CAS#109-76-2;CAT#A802086
Cas No: 109-76-2
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
1,3-Propanediamine
Cas No: 109-76-2
USD $ 1.0-1.0 / Kilogram 1 Kilogram 1000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
1,3-Diaminopropane 109-76-2
Cas No: 109-76-2
USD $ 1.0-1.0 / Kilogram 1 Kilogram 100 Gram/Day Henan Tianfu Chemical Co., Ltd. Contact Supplier

109-76-2 Usage

General Description

Water-white mobile liquid with an odor of amine.

Safety Profile

Poison by ingestion and skin contact. Experimental teratogenic effects. A severe skin and eye irritant. Flammable liquid when exposed to heat, sparks, or flame. When heated to decomposition it emits toxic fumes of NOx. See also AMINES.

Reactivity Profile

1,3-Diaminopropane is heat sensitive. 1,3-Diaminopropane may react with oxidizing agents.

Air & Water Reactions

Highly flammable. Water soluble.

Definition

ChEBI: An alkane-alpha,omega-diamine comprising a propane skeleton with amino substituents at positions 1 and 3.

Health Hazard

ACUTE/CHRONIC HAZARDS: 1,3-Diaminopropane is a strong irritant to eyes and skin: corrosive HAZARDOUS DECOMPOSITION PRODUCTS.

Fire Hazard

1,3-Diaminopropane is a flammable liquid.

Chemical Properties

colourless liquid
InChI:InChI=1/C3H10N2/c4-2-1-3-5/h1-5H2/p+2

109-76-2 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A11932)  1,3-Diaminopropane, 98%    109-76-2 100ml 206.0CNY Detail
Alfa Aesar (A11932)  1,3-Diaminopropane, 98%    109-76-2 500ml 466.0CNY Detail
Alfa Aesar (A11932)  1,3-Diaminopropane, 98%    109-76-2 2500ml 1825.0CNY Detail
Aldrich (D23602)  1,3-Diaminopropane  ≥99% 109-76-2 D23602-25G 322.92CNY Detail
Aldrich (D23602)  1,3-Diaminopropane  ≥99% 109-76-2 D23602-500G 822.51CNY Detail

109-76-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name trimethylenediamine

1.2 Other means of identification

Product number -
Other names 1,3-Diaminopropane

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:109-76-2 SDS

109-76-2Synthetic route

propan-1-ol-3-amine
156-87-6

propan-1-ol-3-amine

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
95%
With ammonia; chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II) In toluene at 135℃; under 26402.6 Torr; for 12h; Autoclave; Inert atmosphere;
With chlorocarbonylhydrido[4,5-bis(dicyclohexylphosphinomethyl)acridine]ruthenium(II); ammonia In toluene at 135℃; under 26402.6 Torr; for 12h; Autoclave; Inert atmosphere;
C19H26N2O2

C19H26N2O2

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With hydrogen; acetic acid In methanol89%
2,2-dimethyl-1,1-bis(2-cyanoethyl)hydrazine
4870-73-9

2,2-dimethyl-1,1-bis(2-cyanoethyl)hydrazine

A

N1-(cyanoethyl)-1,3-propanediamine
35513-93-0

N1-(cyanoethyl)-1,3-propanediamine

B

1,1-dimethyl-2-(3-aminopropyl)hydrazine
22157-84-2

1,1-dimethyl-2-(3-aminopropyl)hydrazine

C

Trimethylenediamine
109-76-2

Trimethylenediamine

D

2,2-dimethyl-1,1-bis(3-aminopropyl)hydrazine
84714-27-2

2,2-dimethyl-1,1-bis(3-aminopropyl)hydrazine

Conditions
ConditionsYield
With hydrogen; nickel In ethanol Catalytic hydrogenation; Further byproducts given;A n/a
B n/a
C n/a
D 66.2%
C12H28CrN5O(2+)

C12H28CrN5O(2+)

A

1,2-di-(3-pyridyl)-ethane
4916-58-9

1,2-di-(3-pyridyl)-ethane

B

3-Methylpyridine
108-99-6

3-Methylpyridine

C

chromium(III) hexahydrate cation
14873-01-9

chromium(III) hexahydrate cation

D

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
In perchloric acid Kinetics; (N2); decompn. of Cr complex in 1 M HClO4 depending on temp. under anaerobic conditions; not isolated, monitored by UV;A 20%
B 65%
C n/a
D n/a
In perchloric acid Kinetics; decompn. of Cr complex in 1 M HClO4 depending on temp. under aerobic conditions; not isolated, monitored by UV;A 38%
B 11%
C n/a
D n/a
1,5-pentanedioic acid
110-94-1

1,5-pentanedioic acid

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With chloroform; tris-(2-chloro-ethyl)-amine; sulfuric acid at 45℃;
2-cyanoethylamine
151-18-8

2-cyanoethylamine

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With sodium-potassium alloy; butan-1-ol
With ammonia; hydrogen; nickel at 90℃; under 88260.9 Torr;
3-azidopropylamine
88192-19-2

3-azidopropylamine

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With hydrogenchloride im CO2-Strom;
With hydrogenchloride; tin(ll) chloride
pentanediamide
3424-60-0

pentanediamide

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With potassium hypobromite at 0 - 60℃;
butanediol bis-(propionitrile)ether
18664-94-3

butanediol bis-(propionitrile)ether

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With ammonia; water; nickel at 100℃; Hydrogenation.unter Druck;
pentanedioyl azide
64624-44-8

pentanedioyl azide

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With hydrogenchloride; ethanol at 100 - 110℃;
1,3-Dichloropropane
142-28-9

1,3-Dichloropropane

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With ethanol; ammonia; water
1,3-dibromo-propane
109-64-8

1,3-dibromo-propane

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With ethanol; ammonia anschl. mit wss. NaOH, dann mit HCl, anschl. mit KOH;
With ethanol; ammonia at 100℃; im Autoklaven;
urea
57-13-6

urea

acrolein
107-02-8

acrolein

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With sodium hydroxide; water; nitric acid at 150℃; under 51485.6 - 73550.8 Torr; Hydrogenation.an Raney-Nickel, anschl. Erwaermen mit NaOH;
acrolein
107-02-8

acrolein

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With ammonia; nickel Hydrogenation.unter Druck;
With methanol; ammonia; water; hydrogen; nickel at 125℃; under 41188.4 - 61782.7 Torr;
With methanol; ammonia; water; hydrogen; nickel at 125℃; under 41188.4 - 61782.7 Torr;
azetidine
503-29-7

azetidine

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With ammonia at 120℃; Rate constant; Mechanism; Thermodynamic data; ΔH(excit.), ΔS(excit.);;
With ammonium hydroxide; perchloric acid at 25℃; Rate constant; Thermodynamic data; E(a), ΔS(excit.);
3-chloropropan-1-amine
14753-26-5

3-chloropropan-1-amine

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With ammonium hydroxide at 50℃; Rate constant; Thermodynamic data; E(a);
Spermine
71-44-3

Spermine

A

N-(3-aminopropyl)-1,4-diaminobutane
124-20-9

N-(3-aminopropyl)-1,4-diaminobutane

B

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With pyrroloquinoline quinone In water at 37℃; examination of PQQ oxidation effect; phosphate buffer (pH=7.2);
N,N-bis(trimethylsilyl)allylamine
7688-51-9

N,N-bis(trimethylsilyl)allylamine

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With sodium hypochlorite; dimethylborane; ammonia 1.) 0 deg C, 1 h, 2.) O deg C; Yield given. Multistep reaction;
(3-aminopropyl)carbamic acid benzyl ester hydrochloride
17400-34-9

(3-aminopropyl)carbamic acid benzyl ester hydrochloride

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In methanol for 4h; Yield given;
N-[1-(4-Hexadecyloxy-phenyl)-meth-(E)-ylidene]-N'-[1-(4-hexadecyloxy-phenyl)-meth-(Z)-ylidene]-propane-1,3-diamine
121511-51-1

N-[1-(4-Hexadecyloxy-phenyl)-meth-(E)-ylidene]-N'-[1-(4-hexadecyloxy-phenyl)-meth-(Z)-ylidene]-propane-1,3-diamine

A

p-n-hexadecyloxybenzaldehyde
59117-18-9

p-n-hexadecyloxybenzaldehyde

B

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With hydrogenchloride; water; cetyltrimethylammonim bromide In chloroform at 25℃; Rate constant;
N-(3-aminopropyl)-1,4-diaminobutane
124-20-9

N-(3-aminopropyl)-1,4-diaminobutane

A

propionaldehyde
123-38-6

propionaldehyde

B

Trimethylenediamine
109-76-2

Trimethylenediamine

C

1,4-diaminobutane
110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With NaPi buffer; oxygen at 37℃; for 0.166667h; catalase and polyamine oxidase presence, pH 6.5, other polyamines and acetylpolyamines, kinetic constants Km (μM) and Vmax (μmol H2O2 formed μg protein-1 min-1);
Spermine
71-44-3

Spermine

A

N-(3-aminopropyl)-1,4-diaminobutane
124-20-9

N-(3-aminopropyl)-1,4-diaminobutane

B

propionaldehyde
123-38-6

propionaldehyde

C

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With NaPi buffer; oxygen at 37℃; for 0.166667h; catalase and polyamine oxidase presence, pH 6.5, other polyamines and acetylpolyamines, kinetic constants Km (μM) and Vmax (μmol H2O2 formed μg protein-1 min-1);
N8-Acetyl-Spermidine
13431-24-8

N8-Acetyl-Spermidine

A

4-(acetylamino)butanal
24431-54-7

4-(acetylamino)butanal

B

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With NaPi buffer; oxygen at 37℃; for 0.166667h; catalase and polyamine oxidase presence, pH 6.5, other polyamines and acetylpolyamines, kinetic constants Km (μM) and Vmax (μmol H2O2 formed μg protein-1 min-1);
N1-Acetyl-Spermidine
14278-49-0

N1-Acetyl-Spermidine

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With NaPi buffer; oxygen at 37℃; for 0.166667h; catalase and polyamine oxidase presence, pH 6.5, other polyamines and acetylpolyamines, kinetic constants Km (μM) and Vmax (μmol H2O2 formed μg protein-1 min-1);
N1-acetylspermine
25593-72-0

N1-acetylspermine

A

Trimethylenediamine
109-76-2

Trimethylenediamine

B

N-(3-acetamidopropyl)-4-aminobutanal

N-(3-acetamidopropyl)-4-aminobutanal

Conditions
ConditionsYield
With KPi buffer; oxygen at 37℃; for 0.166667h; catalase and polyamine oxidase presence, both bound or not bound to hydroxyapatite, other reagent: NaPi buffer, pH 6 or 6.5, other polyamines and acetylpolyamines, kinetic constants Km (μM) and Vmax (μmol H2O2 formed μg protein-1 min-1);
trimethyleneglycol
504-63-2

trimethyleneglycol

A

Trimethylenediamine
109-76-2

Trimethylenediamine

B

propan-1-ol-3-amine
156-87-6

propan-1-ol-3-amine

Conditions
ConditionsYield
With ammonia; hydrogen; Co-Fe catalyst at 195℃; under 37503 - 112509 Torr; Product distribution;
With ammonia; hydrogen; cobalt; iron at 195℃; under 101258 Torr; amination;
With ammonia; hydrogen; Co-La at 190℃; under 101258 Torr; amination;
trimethyleneglycol
504-63-2

trimethyleneglycol

A

bis(3-aminopropyl)amine
56-18-8

bis(3-aminopropyl)amine

B

propan-1-ol
71-23-8

propan-1-ol

C

Trimethylenediamine
109-76-2

Trimethylenediamine

D

propan-1-ol-3-amine
156-87-6

propan-1-ol-3-amine

Conditions
ConditionsYield
With ammonia; hydrogen; carbon monoxide at 210℃; under 101258 Torr; Product distribution; Further Variations:; Catalysts; Temperatures; Pressures; amination;
2-(ethylsulfanyl)pyrimidine
10132-25-9

2-(ethylsulfanyl)pyrimidine

ethanol
64-17-5

ethanol

sodium

sodium

Trimethylenediamine
109-76-2

Trimethylenediamine

5-ethoxy-2-ethylmercapto-3H-pyrimidin-4-one
82153-69-3

5-ethoxy-2-ethylmercapto-3H-pyrimidin-4-one

ethanol
64-17-5

ethanol

sodium

sodium

Trimethylenediamine
109-76-2

Trimethylenediamine

spermine

spermine

A

3-(2,5-dihydro-pyrrol-1-yl)-propylamine
37632-58-9

3-(2,5-dihydro-pyrrol-1-yl)-propylamine

B

Trimethylenediamine
109-76-2

Trimethylenediamine

Conditions
ConditionsYield
With sodium hydroxide; air; copper
Trimethylenediamine
109-76-2

Trimethylenediamine

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

N,N'-ditoluenesulfonyl-1,3-diaminopropane
53364-99-1

N,N'-ditoluenesulfonyl-1,3-diaminopropane

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran; water at 0.2℃; for 3h; Inert atmosphere;100%
at 80℃; for 0.5h;95%
With potassium carbonate In tetrahydrofuran; water at 23℃; for 10h;95%
5-(dimethylamino)naphth-1-ylsulfonyl chloride
605-65-2

5-(dimethylamino)naphth-1-ylsulfonyl chloride

Trimethylenediamine
109-76-2

Trimethylenediamine

N-(3-aminopropyl)-5-(dimethylamino)naphthalene-1-sulfonamide
34987-20-7

N-(3-aminopropyl)-5-(dimethylamino)naphthalene-1-sulfonamide

Conditions
ConditionsYield
In dichloromethane at 0℃; for 4h;100%
In dichloromethane at 20℃; for 18h; Inert atmosphere;99%
In dichloromethane at 0 - 20℃; for 1h;88%
Trimethylenediamine
109-76-2

Trimethylenediamine

acrylonitrile
107-13-1

acrylonitrile

N1,N3-bis(2-cyanoethyl)propane-1,3-diamine
35514-00-2

N1,N3-bis(2-cyanoethyl)propane-1,3-diamine

Conditions
ConditionsYield
In methanol at 20℃; for 16h; Addition; cyanoethylation;100%
at 0℃; for 24h; Darkness;95%
In ethanol at 20℃; for 16h; Addition; cyanoethylation;88%
Trimethylenediamine
109-76-2

Trimethylenediamine

1-phenylbutan-1,3-dione
93-91-4

1-phenylbutan-1,3-dione

(Z)-3-{3-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]propylamino}-1-phenyl-2-buten-1-one
74141-38-1

(Z)-3-{3-[(Z)-1-methyl-3-oxo-3-phenyl-1-propenylamino]propylamino}-1-phenyl-2-buten-1-one

Conditions
ConditionsYield
With silica-supported ferric hydrogensulfate/[Fe(HSO4)3*SiO2] In neat (no solvent) at 20℃; for 0.266667h; regioselective reaction;100%
In ethanol Heating;
thiophene-2-carbaldehyde
98-03-3

thiophene-2-carbaldehyde

Trimethylenediamine
109-76-2

Trimethylenediamine

bis-(2-thenylidene)-trimethylenediamine

bis-(2-thenylidene)-trimethylenediamine

Conditions
ConditionsYield
In ethanol at 20℃; for 4h; Reflux;100%
In ethanol for 1h; Heating;69%
In benzene for 24h; Ambient temperature;
3,4,5-trimethoxy-benzaldehyde
86-81-7

3,4,5-trimethoxy-benzaldehyde

Trimethylenediamine
109-76-2

Trimethylenediamine

N,N'-bis-(3,4,5-trimethoxybenzylidene)-1,3-diaminopropane
126556-34-1

N,N'-bis-(3,4,5-trimethoxybenzylidene)-1,3-diaminopropane

Conditions
ConditionsYield
In methanol for 1h; Ambient temperature;100%
In ethanol for 1h; Heating;59%
In methanol at 20℃;
4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

Trimethylenediamine
109-76-2

Trimethylenediamine

N,N′-bis[(4-methoxyphenyl)methlylidene]propane-1,3-diamine
6958-31-2

N,N′-bis[(4-methoxyphenyl)methlylidene]propane-1,3-diamine

Conditions
ConditionsYield
In ethanol at 20℃; for 4h; Reflux;100%
In ethanol at 20℃; for 4h;96.2%
In methanol for 2h; Reflux;90%
salicylaldehyde
90-02-8

salicylaldehyde

Trimethylenediamine
109-76-2

Trimethylenediamine

N,N'-propane-1,3-diylbis(salicylideneimine)
120-70-7

N,N'-propane-1,3-diylbis(salicylideneimine)

Conditions
ConditionsYield
In ethanol at 20℃; for 4h; Reflux;100%
In methanol at 20℃; for 0.5h;97%
In ethanol97%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

Trimethylenediamine
109-76-2

Trimethylenediamine

N-Boc-1,3-diaminopropane
75178-96-0

N-Boc-1,3-diaminopropane

Conditions
ConditionsYield
In chloroform 1.) 3 h, ice bath, 2.) room temperature, 16 h;100%
In dichloromethane at 0 - 20℃; for 3h; Inert atmosphere;100%
In 1,4-dioxane for 20h; Ambient temperature;98%
2-Hydroxy-5-methylisophthalaldehyde
7310-95-4

2-Hydroxy-5-methylisophthalaldehyde

Trimethylenediamine
109-76-2

Trimethylenediamine

N,N'-propylenebis(3-formyl-5-methylsalicylaldimine)
37512-34-8

N,N'-propylenebis(3-formyl-5-methylsalicylaldimine)

Conditions
ConditionsYield
100%
In isopropyl alcohol at 20℃; for 1h;47%
In ethanol Heating;
Trimethylenediamine
109-76-2

Trimethylenediamine

8-bromo-2',3'-O-isopropylene adenosine
13089-45-7

8-bromo-2',3'-O-isopropylene adenosine

{(3aR,4R,6R,6aR)-6-[6-Amino-8-(3-amino-propylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-methanol
87888-81-1

{(3aR,4R,6R,6aR)-6-[6-Amino-8-(3-amino-propylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-methanol

Conditions
ConditionsYield
In water at 120℃;100%
Trimethylenediamine
109-76-2

Trimethylenediamine

acetone
67-64-1

acetone

6,6-dimethyl-1,5-diazabicyclo<3.1.0>hexane
104518-69-6

6,6-dimethyl-1,5-diazabicyclo<3.1.0>hexane

Conditions
ConditionsYield
With sodium hypochlorite In water at -5 - 20℃; for 13h;100%
With sodium hydroxide; sodium hypochlorite In water at 20℃; for 6h;80%
With sodium hypochlorite In water at 0 - 5℃;
With tert-butylhypochlorite In methanol at -5 - 5℃; for 24h;
Trimethylenediamine
109-76-2

Trimethylenediamine

ethyl 2-cyanoacetate
105-56-6

ethyl 2-cyanoacetate

2-cyano-N-[3-(2-cyanoacetylamino)propyl]acetamide
111233-69-3

2-cyano-N-[3-(2-cyanoacetylamino)propyl]acetamide

Conditions
ConditionsYield
100%
for 24h; Ambient temperature;90%
at 20℃; for 1h;88%
Trimethylenediamine
109-76-2

Trimethylenediamine

6,7-Dimethoxy-naphthalene-2-carboxylic acid pentafluorophenyl ester

6,7-Dimethoxy-naphthalene-2-carboxylic acid pentafluorophenyl ester

1,3-bis(6,7-dimethoxy-2-naphthalenecarboxamido)propane

1,3-bis(6,7-dimethoxy-2-naphthalenecarboxamido)propane

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 70℃;100%
11-chloro-10H-indolo-[3,2-b]quinoline
80271-19-8

11-chloro-10H-indolo-[3,2-b]quinoline

Trimethylenediamine
109-76-2

Trimethylenediamine

N1-(10H-indolo[3,2-b]quinolin-11-yl)propane-1,3-diamine
188630-48-0

N1-(10H-indolo[3,2-b]quinolin-11-yl)propane-1,3-diamine

Conditions
ConditionsYield
With hydrogenchloride In 2-ethoxy-ethanol for 15h; Heating;100%
Stage #1: 11-chloro-10H-indolo-[3,2-b]quinoline; Trimethylenediamine With hydrogenchloride In 2-ethoxy-ethanol; water for 17h; Reflux;
Stage #2: With potassium hydroxide In 2-ethoxy-ethanol; water Cooling with ice;
75.7%
(-)-dimethy-2,3-O-isopropylidene-L-tartrate
37031-29-1

(-)-dimethy-2,3-O-isopropylidene-L-tartrate

Trimethylenediamine
109-76-2

Trimethylenediamine

(4R,5R)-2,2-Dimethyl-[1,3]dioxolane-4,5-dicarboxylic acid bis-[(3-amino-propyl)-amide]
197906-38-0

(4R,5R)-2,2-Dimethyl-[1,3]dioxolane-4,5-dicarboxylic acid bis-[(3-amino-propyl)-amide]

Conditions
ConditionsYield
In methanol for 216h; Ambient temperature;100%
4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane
57280-22-5

4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane

Trimethylenediamine
109-76-2

Trimethylenediamine

C17H34N2O6

C17H34N2O6

Conditions
ConditionsYield
In ethanol epoxide:amine=2:1;100%
Trimethylenediamine
109-76-2

Trimethylenediamine

(2S,4R)-4-(methanesulfonyloxy)-2-[(methanesulfonyloxy)methyl]pyrrolidine-1-carboxylic acid tert-butyl ester
133628-17-8

(2S,4R)-4-(methanesulfonyloxy)-2-[(methanesulfonyloxy)methyl]pyrrolidine-1-carboxylic acid tert-butyl ester

(1S,4S)-5-(3-aminopropyl)-2-(tert-butoxycarbonyl)-2,5-diazabicyclo[2.2.1]heptane
191280-84-9

(1S,4S)-5-(3-aminopropyl)-2-(tert-butoxycarbonyl)-2,5-diazabicyclo[2.2.1]heptane

Conditions
ConditionsYield
4 h, 60 deg C, 8 h;100%
Trimethylenediamine
109-76-2

Trimethylenediamine

(4S,5S)-2,2-Dimethyl-[1,3]dioxolane-4,5-dicarboxylic acid bis-[(3-amino-propyl)-amide]

(4S,5S)-2,2-Dimethyl-[1,3]dioxolane-4,5-dicarboxylic acid bis-[(3-amino-propyl)-amide]

Conditions
ConditionsYield
at 20℃; for 5.5h; Acylation;100%
at 20℃; for 5.5h;
4,7-dichloroquinoline
86-98-6

4,7-dichloroquinoline

Trimethylenediamine
109-76-2

Trimethylenediamine

N-(7-chloroquinolin-4-yl)propane-1,3-diamine
7597-14-0

N-(7-chloroquinolin-4-yl)propane-1,3-diamine

Conditions
ConditionsYield
In neat (no solvent) at 110℃;100%
Inert atmosphere;100%
In isopropyl alcohol at 100℃; for 20h;98%
5-hexynoic acid ethyl ester
108545-38-6

5-hexynoic acid ethyl ester

Trimethylenediamine
109-76-2

Trimethylenediamine

N-(3-aminopropyl)hex-5-ynamide
398507-42-1

N-(3-aminopropyl)hex-5-ynamide

Conditions
ConditionsYield
at 60℃; for 48h;100%
(3aS,4S,6R,6aS)-2,2-dimethyl-6-vinyltetrahydrofuro[3,4-d][1,3]dioxol-4-ol
73111-64-5

(3aS,4S,6R,6aS)-2,2-dimethyl-6-vinyltetrahydrofuro[3,4-d][1,3]dioxol-4-ol

Trimethylenediamine
109-76-2

Trimethylenediamine

hexahydro-2-[[D-lyxo-3-hydroxy-1,2-[(1-methylethylidene)bis(oxy)]-4-pentenyl]]pyrimidine

hexahydro-2-[[D-lyxo-3-hydroxy-1,2-[(1-methylethylidene)bis(oxy)]-4-pentenyl]]pyrimidine

Conditions
ConditionsYield
100%
Trimethylenediamine
109-76-2

Trimethylenediamine

3β-(4'-chlorophenyl)tropane-2β-carboxylic acid

3β-(4'-chlorophenyl)tropane-2β-carboxylic acid

1,3-di-(3β-(p-chlorophenyl)tropane-2β-carboxamide)-propane

1,3-di-(3β-(p-chlorophenyl)tropane-2β-carboxamide)-propane

Conditions
ConditionsYield
Stage #1: 3β-(4'-chlorophenyl)tropane-2β-carboxylic acid With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine In dichloromethane at 0℃; for 0.166667h;
Stage #2: Trimethylenediamine In dichloromethane at 20℃;
100%
Trimethylenediamine
109-76-2

Trimethylenediamine

N-carboxyethylchitin ethyl ester; Mn=12000, Mw=49000, degree of CO2Et substitution per sugar unit =1.17

N-carboxyethylchitin ethyl ester; Mn=12000, Mw=49000, degree of CO2Et substitution per sugar unit =1.17

N-carboxyethylchitin 3-aminopropylamide

N-carboxyethylchitin 3-aminopropylamide

Conditions
ConditionsYield
In ethanol; water at 70℃; for 24h;100%
acetoacetic acid methyl ester
105-45-3

acetoacetic acid methyl ester

Trimethylenediamine
109-76-2

Trimethylenediamine

3-[3-(2-methoxycarbonyl-1-methylvinylamino)-propylamino]but-2-enoic acid methyl ester

3-[3-(2-methoxycarbonyl-1-methylvinylamino)-propylamino]but-2-enoic acid methyl ester

Conditions
ConditionsYield
With silica-supported ferric hydrogensulfate/[Fe(HSO4)3*SiO2] In neat (no solvent) at 20℃; for 0.2h; regioselective reaction;100%
zirconium(IV) chloride at 20℃; for 0.25h;95%
With sulfated zirconia at 20℃; for 0.416667h;92%
(3α,5β)-3,24-bis(3-bromophenoxy)cholane
874306-28-2

(3α,5β)-3,24-bis(3-bromophenoxy)cholane

Trimethylenediamine
109-76-2

Trimethylenediamine

N1-[3-((R)-4-{(3S,5R,8R,9S,10S,13R,14S,17R)-3-[3-(3-Amino-propylamino)-phenoxy]-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl}-pentyloxy)-phenyl]-propane-1,3-diamine
874306-46-4

N1-[3-((R)-4-{(3S,5R,8R,9S,10S,13R,14S,17R)-3-[3-(3-Amino-propylamino)-phenoxy]-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl}-pentyloxy)-phenyl]-propane-1,3-diamine

Conditions
ConditionsYield
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane Heating;100%
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; [Pd(dibenzylideneacetone)2] In 1,4-dioxane for 5h; Heating;60 % Spectr.
Trimethylenediamine
109-76-2

Trimethylenediamine

9-anthracene aldehyde
642-31-9

9-anthracene aldehyde

N-((anthracen-10-Yl)methylene)-N′-((anthracen-9-Yl)methylene)propane-1,3-diamine

N-((anthracen-10-Yl)methylene)-N′-((anthracen-9-Yl)methylene)propane-1,3-diamine

Conditions
ConditionsYield
With acetic acid In ethanol Heating;100%
In methanol; N,N-dimethyl-formamide for 4h; Heating;94%
With acetic acid In methanol for 12h; Reflux;85.32%
C18H33O2N
251349-29-8

C18H33O2N

Trimethylenediamine
109-76-2

Trimethylenediamine

C20H39ON3
1026288-30-1

C20H39ON3

Conditions
ConditionsYield
In methanol at 20℃; for 120h;100%
C18H33NO2

C18H33NO2

Trimethylenediamine
109-76-2

Trimethylenediamine

C20H39N3O

C20H39N3O

Conditions
ConditionsYield
In methanol at 20℃; for 72h;100%
titanium
7440-32-6

titanium

phosphoric acid
86119-84-8, 7664-38-2

phosphoric acid

water
7732-18-5

water

Trimethylenediamine
109-76-2

Trimethylenediamine

Ti2(PO4)(HPO4)2*(water)2*0.5(1,3-diaminopropane)

Ti2(PO4)(HPO4)2*(water)2*0.5(1,3-diaminopropane)

Conditions
ConditionsYield
In neat (no solvent) Ti:1,3-diaminopropane:H3PO4:H2O ratio = 2:2.21:13.65:500, autoclave, pH=2, 170°C (1 d, autogenous pressure); washing (water, alcohol and acetone); elem. anal.;100%
With boric acid; HF In neat (no solvent) Ti:boric acid:H3PO4:1,3-diaminopropane:HF:H2O ratio = 1:6.54:13.65:2.21:3.36:600;

109-76-2Upstream product

109-76-2Related news

Research articleModification of multi-walled carbon nanotubes by 1,3-Diaminopropane (cas 109-76-2) to increase CO2 adsorption capacity08/19/2019

Greenhouse gas emissions have increased dramatically over the past years and had a significant impact on global warming. This study investigates the modification of multi-walled carbon nanotubes (MWCNTs) with diamine precursor to improve the carbon dioxide adsorption capacity. To achieve this go...detailed

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