A convenient procedure for the preparation of 5,6-dihydro-6-nitro-5-phenylfuro[2,3-d]pyrimidin-4(3H)-ones and 5-phenylfuro[2,3-d]pyrimidin-4(3H)-ones

DOI: 10.1016/S0040-4020(01)92249-5

Source and publish data:

Tetrahedron p. 3069 - 3080 (1992)

Update date:2022-07-30

Topics: Synthesis Yield Chromatography Recrystallization Nucleophilic substitution Pyrimidine Cyclization Catalysis Reaction Optimization Electrophilic Aromatic Substitution Spectroscopic Analysis Furan Heterocyclic compound Nitro group (–NO?)

Authors:

Dauzonne, Daniel

Adam-Launay, Anne

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Article abstract of DOI:10.1016/S0040-4020(01)92249-5

The triethylamine-promoted condensation of Z-(2-chloro-2-nitroethenyl)benzenes with 4,6-dihydroxypyrimidine provides 5,6-dihydro-6-nitro-5-phenylfuro[2,3-d]pyrimidin-4(3H)-ones at room temperature. Involving the same starting materials, but using DBU in r

Full text of DOI:10.1016/S0040-4020(01)92249-5

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Product name:Furo[2,3-d]pyrimidin-4(1H)-one, 5-(4-nitrophenyl)-

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