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N,N'-Methylenebisacrylamide suppliers in China
Cas No: 110-26-9
No Data 100 Gram 1-1000 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High pun n-methylenebisacrylamide with high quality and best price cas:110-26-9
Cas No: 110-26-9
USD $ 10.0-20.0 / Kilogram 1 Kilogram 99999 Kilogram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
N,N'-Methylenebisacrylamide 110-26-9
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No Data 1 Metric Ton 3 Metric Ton/Day Zouping Mingxing Chemical Co.,Ltd. Contact Supplier
N,N'-Methylenebisacrylamide
Cas No: 110-26-9
USD $ 20.0-30.0 / Gram 10 Gram 200 Metric Ton/Year Jinan Finer Chemical Co., Ltd Contact Supplier
N,N'-Methylenebisacrylamide cas:110-26-9
Cas No: 110-26-9
No Data 1 Kilogram 100 Metric Ton/Day Henan Tianfu Chemical Co., Ltd. Contact Supplier
Low price with good quality N,N'-METHYLENESBISACRYLAMIDE
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No Data No Data 5 Metric Ton/Day Lonwin Chemical Group Limited Contact Supplier
High quality n,n'-methylene-bis-acrylamide (mba) supplier in China
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No Data 1 Kilogram 600 Metric Ton/Year Simagchem Corporation Contact Supplier
N,N'-Methylenebisacrylamide suppliers in China CAS NO.110-26-9
Cas No: 110-26-9
USD $ 1.0-3.0 / Metric Ton 1 Metric Ton 10 Metric Ton/Day Hebei yanxi chemical co.,LTD. Contact Supplier
MBA N N'-Methylenebisacrylamide 110-26-9
Cas No: 110-26-9
No Data 1 Metric Ton 500 Metric Ton/Day Hefei TNJ chemical industry co.,ltd Contact Supplier
N,N'-Methylenebisacrylamide
Cas No: 110-26-9
No Data 1 Kilogram 20 Metric Ton/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier

110-26-9 Usage

Chemical Properties

white crystalline powder

Uses

Organic intermediate, cross-linking agent.

Uses

N,N-Methylene-bis-acrylamide is an organic intermediate; cross-linking agent for preparation of polyacrylamides; in preparing poly-acrylamide gel for e1ectrophoresis, chemical grouting and other purposes; in NAPP and Nyloprint UV-cured printing plates.

Uses

N,N'-Methylenebisacrylamide is used in the preparation of polyacrylamide gels for electrophoretic separation of nucleic acids and proteins. It has also been used as a test compound for studying the biochemical isolation of insoluble Tau in transgenic mouse models of tauopathy by examining the two main isolation methods sarkosyl and formic acid extraction.

General Description

White crystalline powder with a neutral odor.

Air & Water Reactions

Very slightly water soluble.

Reactivity Profile

N,N'-Methylenebisacrylamide is incompatible with strong oxidizers, strong acids and strong bases.

Hazard

Toxic by ingestion.

Fire Hazard

Flash point data for N,N'-Methylenebisacrylamide are not available; however, N,N'-Methylenebisacrylamide is probably combustible.

Safety Profile

Poison by ingestion. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of NOx.

Purification Methods

Recrystallise the amide from MeOH (100g dissolved in 500mL boiling MeOH) and filter without suction in a warmed funnel. Allow to stand at room temperature and then at -15oC overnight. The crystals are collected with suction in a cooled funnel and washed with cold MeOH. The crystals are air-dried in a warm oven. [Beilstein 2 IV 1472.] VERY TOXIC (neurotoxic).

110-26-9 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (L04694)  N,N'-Methylenebisacrylamide, 97%    110-26-9 100g 230.0CNY Detail
Alfa Aesar (L04694)  N,N'-Methylenebisacrylamide, 97%    110-26-9 500g 764.0CNY Detail
Alfa Aesar (43701)  N,N'-Methylenebisacrylamide, 99+%    110-26-9 25g 315.0CNY Detail
Alfa Aesar (43701)  N,N'-Methylenebisacrylamide, 99+%    110-26-9 100g 1137.0CNY Detail

110-26-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name N,N'-Methylenebisacrylamide

1.2 Other means of identification

Product number -
Other names N,N'-Methylenediacrylamide

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:110-26-9 SDS

110-26-9Synthetic route

formaldehyd
50-00-0

formaldehyd

2-propenamide
79-06-1

2-propenamide

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone In water at 65 - 75℃; for 2.5h; Reagent/catalyst; Temperature;87.54%
N-Methylolacrylamid
924-42-5

N-Methylolacrylamid

1,2-dichloro-ethane
107-06-2

1,2-dichloro-ethane

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Conditions
ConditionsYield
With hydrogenchloride
formaldehyd
50-00-0

formaldehyd

1,2-dichloro-ethane
107-06-2

1,2-dichloro-ethane

2-propenamide
79-06-1

2-propenamide

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Conditions
ConditionsYield
With hydrogenchloride
formaldehyd
50-00-0

formaldehyd

acrylonitrile
107-13-1

acrylonitrile

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Conditions
ConditionsYield
With sulfuric acid; water
With hydroquinone
With sulfuric acid
formaldehyd
50-00-0

formaldehyd

sulfuric acid
7664-93-9

sulfuric acid

acrylonitrile
107-13-1

acrylonitrile

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Pentaerythritol
115-77-5

Pentaerythritol

N-Methylolacrylamid
924-42-5

N-Methylolacrylamid

A

etherbis-N-methylenacrylamide

etherbis-N-methylenacrylamide

B

C13H22N2O6
85030-50-8

C13H22N2O6

C

C14H27NO8

C14H27NO8

D

C17H27N3O7

C17H27N3O7

E

C26H42N4O11

C26H42N4O11

F

C30H47N5O12

C30H47N5O12

G

C34H52N6O13

C34H52N6O13

H

C26H42N4O11

C26H42N4O11

I

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Conditions
ConditionsYield
Stage #1: Pentaerythritol; N-Methylolacrylamid With tempol; toluene-4-sulfonic acid In methanol at 86℃; for 1.5h;
Stage #2: With ammonia In methanol; propyleneglycol monomethylether; water
p-(1,4,7,10,13-Pentaoxatetradecyl)benzylacetal-bisacrylamide

p-(1,4,7,10,13-Pentaoxatetradecyl)benzylacetal-bisacrylamide

acryloyl chloride
814-68-6

acryloyl chloride

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Conditions
ConditionsYield
With sodium hydroxide; potassium carbonate; triethylamine In 1,4-dioxane; methanol; water; ethyl acetate200 mg (58%)
propylene glycol
57-55-6

propylene glycol

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

bis(mesityleneformyl)phosphine
139031-06-4

bis(mesityleneformyl)phosphine

N,N-methylene(bis(bis(2,4,6-trimethylbenzoyl)phosphino)propanamide)
1591653-06-3

N,N-methylene(bis(bis(2,4,6-trimethylbenzoyl)phosphino)propanamide)

Conditions
ConditionsYield
With triethylamine In 1,2-dimethoxyethane; toluene at 50℃; for 12h; Schlenk technique; Inert atmosphere;99%
N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetra[4-(2-aminoethyl)phenoxy]perylene-3,4,9,10-tetracarboxylic acid diimide
347371-56-6

N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetra[4-(2-aminoethyl)phenoxy]perylene-3,4,9,10-tetracarboxylic acid diimide

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

C136H158N22O24
1549684-13-0

C136H158N22O24

Conditions
ConditionsYield
In methanol; water at 50℃; for 48h; Michael Addition; Inert atmosphere;95%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

acrylic acid
79-10-7

acrylic acid

poly(acrylic acid), cross-linked by 0.15 wt % of N,N'-methylenebisacrylamide, neutralized with degree of neutralization 0.3; monomer(s): acrylic acid; N,N'-methylenebisacrylamide

poly(acrylic acid), cross-linked by 0.15 wt % of N,N'-methylenebisacrylamide, neutralized with degree of neutralization 0.3; monomer(s): acrylic acid; N,N'-methylenebisacrylamide

Conditions
ConditionsYield
With ammonium persulfate; N,N,N,N,-tetramethylethylenediamine In water at 30℃; for 1h;93%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

4-sulfanylphenol
637-89-8

4-sulfanylphenol

methylene bis[3-(4-hydroxyphenylsulfanyl)propanecarboxamide]

methylene bis[3-(4-hydroxyphenylsulfanyl)propanecarboxamide]

Conditions
ConditionsYield
With triethylamine at 20℃; for 24h; Michael Addition;93%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

dimethyl acetylenedicarboxylate
762-42-5

dimethyl acetylenedicarboxylate

triethyl phosphite
122-52-1

triethyl phosphite

dimethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diethylphosphono)succinate

dimethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diethylphosphono)succinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 5.25h; diastereoselective reaction;92%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

ammonium thiocyanate
1147550-11-5

ammonium thiocyanate

benzenediazonium tetrafluoroborate
369-57-3

benzenediazonium tetrafluoroborate

N-[(3-phenyl-2-thiocyanatopropionylamino)methyl]acrylamide

N-[(3-phenyl-2-thiocyanatopropionylamino)methyl]acrylamide

Conditions
ConditionsYield
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 10 - 15℃; for 1.25h;91%
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 10 - 15℃; for 0.75h;91%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

trisodium (S,S)-ethylenediamine-N,N’-disuccinic acid
178949-82-1

trisodium (S,S)-ethylenediamine-N,N’-disuccinic acid

BA-EDDS

BA-EDDS

Conditions
ConditionsYield
With lithium hydroxide at 20℃; for 48h;90.1%
1,4,8,11-Tetraazacyclotetradecane
295-37-4

1,4,8,11-Tetraazacyclotetradecane

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

3-(1,4,8,11tetraaza-cyclotetradec-1-yl)-N-[(3-1,4,8,11tetraaza-cyclotetradec-1-yl-propionylamino)-methyl]-propionamide

3-(1,4,8,11tetraaza-cyclotetradec-1-yl)-N-[(3-1,4,8,11tetraaza-cyclotetradec-1-yl-propionylamino)-methyl]-propionamide

Conditions
ConditionsYield
With 2,4-di-tert-Butylphenol; toluene-4-sulfonic acid In chloroform Ambient temperature; 2-4d;90%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

ammonium thiocyanate
1147550-11-5

ammonium thiocyanate

2,5-dichloroaniline diazonium fluoroboric salt

2,5-dichloroaniline diazonium fluoroboric salt

N-{[3-(2,5-dichloro-phenyl)-2-thiocyanato-propionylamino]-methyl}-acrylamide

N-{[3-(2,5-dichloro-phenyl)-2-thiocyanato-propionylamino]-methyl}-acrylamide

Conditions
ConditionsYield
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 10 - 15℃;90%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

acetylenedicarboxylic acid diethyl ester
762-21-0

acetylenedicarboxylic acid diethyl ester

phosphorous acid trimethyl ester
121-45-9

phosphorous acid trimethyl ester

diethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(dimethyphosphono)succinate

diethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(dimethyphosphono)succinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 5.25h; diastereoselective reaction;90%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

N-Isopropylacrylamide
2210-25-5

N-Isopropylacrylamide

N-propylacrylamide
25999-13-7

N-propylacrylamide

4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole
627546-76-3

4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole

polymer, emulsion polymerization; Monomer(s): N-isopropylacrylamide, 75 mM; N-n-propylacrylamide, 25 mM; N,N\-methylenebisacrylamide, 1 mM; 4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole, 0.1 mM

polymer, emulsion polymerization; Monomer(s): N-isopropylacrylamide, 75 mM; N-n-propylacrylamide, 25 mM; N,N\-methylenebisacrylamide, 1 mM; 4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole, 0.1 mM

Conditions
ConditionsYield
With ammonium persulfate; N,N,N,N,-tetramethylethylenediamine; sodium dodecyl-sulfate at 70℃; for 4h;88.3%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

dimethyl acetylenedicarboxylate
762-42-5

dimethyl acetylenedicarboxylate

phosphorous acid trimethyl ester
121-45-9

phosphorous acid trimethyl ester

dimethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(dimethylphosphono)succinate

dimethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(dimethylphosphono)succinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 5.25h; diastereoselective reaction;87%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

potassium thioacyanate
333-20-0

potassium thioacyanate

benzenediazonium tetrafluoroborate
369-57-3

benzenediazonium tetrafluoroborate

N,N-methylenebis(2-thiocyanato-3-phenylpropionamide)

N,N-methylenebis(2-thiocyanato-3-phenylpropionamide)

Conditions
ConditionsYield
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 15℃; for 1.75h;86%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

4-methoxybenzenediazonium tetrafluoroborate
459-64-3

4-methoxybenzenediazonium tetrafluoroborate

ammonium thiocyanate
1147550-11-5

ammonium thiocyanate

N-{[3-(4-methoxy-phenyl)-2-thiocyanato-propionylamino]-methyl}-acrylamide
524067-02-5

N-{[3-(4-methoxy-phenyl)-2-thiocyanato-propionylamino]-methyl}-acrylamide

Conditions
ConditionsYield
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 10 - 15℃;85%
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 10 - 15℃;85%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

ammonium thiocyanate
1147550-11-5

ammonium thiocyanate

4-methylbenzenediazonium tetrafluoroborate
459-44-9

4-methylbenzenediazonium tetrafluoroborate

N-[(2-thiocyanato-3-p-tolyl-propionylamino)-methyl]-acrylamide
524067-01-4

N-[(2-thiocyanato-3-p-tolyl-propionylamino)-methyl]-acrylamide

Conditions
ConditionsYield
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 10 - 15℃;85%
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 10 - 15℃;85%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

acrylic acid
79-10-7

acrylic acid

poly(acrylic acid), cross-linked by 0.2 wt % of N,N'-methylenebisacrylamide, neutralized with degree of neutralization 0.4; monomer(s): acrylic acid; N,N'-methylenebisacrylamide

poly(acrylic acid), cross-linked by 0.2 wt % of N,N'-methylenebisacrylamide, neutralized with degree of neutralization 0.4; monomer(s): acrylic acid; N,N'-methylenebisacrylamide

Conditions
ConditionsYield
With ammonium persulfate; N,N,N,N,-tetramethylethylenediamine In water at 50℃; for 1h;85%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Di-tert-butyl acetylenedicarboxylate
66086-33-7

Di-tert-butyl acetylenedicarboxylate

phosphorous acid trimethyl ester
121-45-9

phosphorous acid trimethyl ester

di-tert-butyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(dimethyphosphono)succinate

di-tert-butyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(dimethyphosphono)succinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 5.25h; diastereoselective reaction;85%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

N-Isopropylacrylamide
2210-25-5

N-Isopropylacrylamide

4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole
627546-76-3

4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole

polymer, emulsion polymerization; Monomer(s): N-isopropylacrylamide, 100 mM; N,N\-methylenebisacrylamide, 1 mM; 4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole, 0.1 mM

polymer, emulsion polymerization; Monomer(s): N-isopropylacrylamide, 100 mM; N,N\-methylenebisacrylamide, 1 mM; 4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole, 0.1 mM

Conditions
ConditionsYield
With ammonium persulfate; N,N,N,N,-tetramethylethylenediamine; sodium dodecyl-sulfate at 70℃; for 4h;84.9%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

N-isopropylmethacrylamide
13749-61-6

N-isopropylmethacrylamide

4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole
627546-76-3

4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole

polymer, emulsion polymerization; Monomer(s): N-isopropylmethacrylamide, 100 mM; N,N\-methylenebisacrylamide, 1 mM; 4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole, 0.1 mM

polymer, emulsion polymerization; Monomer(s): N-isopropylmethacrylamide, 100 mM; N,N\-methylenebisacrylamide, 1 mM; 4-N-(2-acryloyloxyethyl)-N-methylamino-7-N,N-dimethylaminosulfonyl-2,1,3-benzoxadiazole, 0.1 mM

Conditions
ConditionsYield
With ammonium persulfate; N,N,N,N,-tetramethylethylenediamine; sodium dodecyl-sulfate at 70℃; for 4h;84.9%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

2-propenamide
79-06-1

2-propenamide

polymer; monomer(s): acrylamide; N,N\-methylenebis(acrylamide)

polymer; monomer(s): acrylamide; N,N\-methylenebis(acrylamide)

Conditions
ConditionsYield
With ammonium persulfate; N,N,N,N,-tetramethylethylenediamine In various solvent(s) at 65℃; Product distribution; Further Variations:; Solvents; Temperatures;84%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Di-tert-butyl acetylenedicarboxylate
66086-33-7

Di-tert-butyl acetylenedicarboxylate

triethyl phosphite
122-52-1

triethyl phosphite

di-tert-butyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diethylphosphono)succinate

di-tert-butyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diethylphosphono)succinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 5.25h; diastereoselective reaction;84%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

2-methyl-acrylic acid 3-dimethylamino-propyl amide
5205-93-6

2-methyl-acrylic acid 3-dimethylamino-propyl amide

2-propenamide
79-06-1

2-propenamide

(3-acrylamidophenyl)boronic acid
99349-68-5

(3-acrylamidophenyl)boronic acid

copolymer; monomer(s): 3-acrylamidophenylboronic acid; N-(3-dimethylaminopropyl)methacrylamide; N,N'-methylenebisacrylamide; acrylamide

copolymer; monomer(s): 3-acrylamidophenylboronic acid; N-(3-dimethylaminopropyl)methacrylamide; N,N'-methylenebisacrylamide; acrylamide

Conditions
ConditionsYield
With α,α'-azodiizobutyramidine-dihydrochloride In water; dimethyl sulfoxide at 60℃; for 20h;83.7%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

2-methylphenyl diazonium tetrafluoroborate
2093-46-1

2-methylphenyl diazonium tetrafluoroborate

ammonium thiocyanate
1147550-11-5

ammonium thiocyanate

N-[(2-thiocyanato-3-o-tolyl-propionylamino)-methyl]-acrylamide

N-[(2-thiocyanato-3-o-tolyl-propionylamino)-methyl]-acrylamide

Conditions
ConditionsYield
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 10 - 15℃;82%
triphenyl phosphite
101-02-0

triphenyl phosphite

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

Di-tert-butyl acetylenedicarboxylate
66086-33-7

Di-tert-butyl acetylenedicarboxylate

di-tert-buthyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diphenylphosphono)succinate

di-tert-buthyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diphenylphosphono)succinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 5.25h; diastereoselective reaction;82%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

potassium thioacyanate
333-20-0

potassium thioacyanate

2,5-dichloroaniline diazonium fluoroboric salt

2,5-dichloroaniline diazonium fluoroboric salt

3-(2,5-dichloro-phenyl)-N-{[3-(2,5-dichloro-phenyl)-2-thiocyanato-propionylamino]-methyl}-2-thiocyanato-propionamide

3-(2,5-dichloro-phenyl)-N-{[3-(2,5-dichloro-phenyl)-2-thiocyanato-propionylamino]-methyl}-2-thiocyanato-propionamide

Conditions
ConditionsYield
With copper(II) bis(tetrafluoroborate) In water; N,N-dimethyl-formamide at 15℃;81%
N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

acetylenedicarboxylic acid diethyl ester
762-21-0

acetylenedicarboxylic acid diethyl ester

triethyl phosphite
122-52-1

triethyl phosphite

dethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diethylphosphono)succinate

dethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diethylphosphono)succinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 5.25h; diastereoselective reaction;81%
triphenyl phosphite
101-02-0

triphenyl phosphite

N,N'-Methylenebisacrylamide
110-26-9

N,N'-Methylenebisacrylamide

acetylenedicarboxylic acid diethyl ester
762-21-0

acetylenedicarboxylic acid diethyl ester

diethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diphenylphosphono)succinate

diethyl 2-[acryloyl(acryloylaminomethyl)amino]-3-(diphenylphosphono)succinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 5.25h; diastereoselective reaction;80%
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