Heteronuclear Cluster Formation: The Synthesis and Structure of the Chloro-bridged Tetranuclear Complex aneS3)>2(PF6)2 Incorporating a Ladder (aneS3 = 1,4,7-Trithiacyclononane)

DOI: 10.1039/c39920000848

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 848 - 850 (1992)

Update date:2022-07-30

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Authors:

Blake, Alexander J.

Christie, Robert M.

Roberts, Yvonne V.

Sullivan, Martin J.

Schroeder, Martin

Yellowlees, Lesley J.

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Article abstract of DOI:10.1039/c39920000848

Treatment of aneS3)>, formed in high yield by reaction of with <9>aneS3, with TlPF6 in CH2Cl2 at 273 K affords the yellow hetero-cluster species aneS3)>2(PF6)2 incorporating a ladder; dissolution of aneS3)>2(PF6)2 in acetone leads to precipitation of TlCl and the formation of the orange chloro-bridged dimer aneS3)>2(PF6)2.

Full text of DOI:10.1039/c39920000848

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