Erratum: Iridium-catalyzed hydrogen transfer: Synthesis of substituted benzofurans, benzothiophenes, and indoles from benzyl alcohols (Organic Letters (2013) 15 (15) (3876-3879) DOI: 10.1021/ol401610e)

Full text of DOI:10.1021/ol500762n

Addition/Correction
pubs.acs.org/OrgLett
Correction to Iridium-Catalyzed Hydrogen Transfer: Synthesis of
Substituted Benzofurans, Benzothiophenes, and Indoles from Benzyl
Alcohols
Bruno Anxionnat, Domingo Gomez Pardo, Gino Ricci, Kai Rossen, and Janine Cossy*
Org. Lett. 2013, 15 (15), 3876−3879. DOI: 10.1021/ol401610e
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* Supporting Information
n the Supporting Information of this paper, the presence of
solvents was observed in the spectra of 8, 12e, 12f, 15a, and
16c. Original products were found in our library, and the
spectra were rerecorded and have been replaced for compounds
8, 12e,f, 15a, and 16c.
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The spectra for 2, 6, 9, 10, 11b,c, 12c,d, 13a,b, 14a,e,f,
15b,c−e, 16a,b, 17b−d, 18b, 20b−d, 21a,b, and 22a−d were
found to be edited to remove solvents and impurities. Original
products were located and purified, and the spectra were
recorded and have been replaced for all of the above
compounds except for 2, 18b, and 22b,d, which were
resynthesized and new spectra are provided. In addition, for
16a, the original FID file was located and the correct spectra are
provided. Except as stated below, yields remained as previously
reported.
In Scheme 4, compound 2 (volatile) was resynthesized, and
the yield was found to be 53%.
In Scheme 6, compound 18b was resynthesized, and the
yield was found to be 62%. For compound 18b, a note should
be added: 48 h at 110 °C were necessary to perform a complete
reaction.
In Scheme 7, compounds 22b and 22d were resynthesized.
The yield for 22b was found to be 65%, and the yield for 22d
was found to be 62%.
ASSOCIATED CONTENT
* Supporting Information
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Revised file containing experimental data and spectra. This
material is available free of charge via the Internet at http://
pubs.acs.org.
Published: April 18, 2014
© 2014 American Chemical Society
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dx.doi.org/10.1021/ol500762n | Org. Lett. 2014, 16, 2297−2297