Evaluation of the final deprotection system for the solid-phase synthesis of tyr(SO3H)-containing peptides with 9-fluorenylmethyloxycarbonyl (Fmoc)-strategy and its application to the synthesis of cholecystokinin (CCK)-12

DOI: 10.1248/cpb.41.376

Source and publish data:

Chemical and Pharmaceutical Bulletin p. 376 - 380 (1993)

Update date:2022-08-04

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Authors:

Yagami Yagami

Shiwa Shiwa

Futaki Futaki

Kitagawa

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Article abstract of DOI:10.1248/cpb.41.376

Acidolytic deprotection and cleavage conditions for an acid-labile Tyr(SO₃H)-containing peptide were systematically examined with respect to acid, temperature, and scavenger. The 90% aqueous trifluoroacetic acid (TFA)-based reagent systems (90%

Full text of DOI:10.1248/cpb.41.376

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