Recueil des Travaux Chimiques des Pays-Bas p. 464 - 466 (1993)
Update date:2022-08-04
Topics:
Verduyn, R.
Klein, P. A. M. van der
Douwes, M.
Marel, G. A. van der
Boom, J. H. van
An efficient synthesis of methyl heptaglucoside 2 using poly(ethyleneglycol)monomethyl ether as a polymer support is described.Elongation of the acceptor 11, anchored via a succinoyl linkage to PEG, with the appropriate glycosyl donors 4-6 and intermittent protective group manipulations gave fully protected heptamer 18.Deprotection of 18 furnished, after purification as its peracetate, title compound 2 in a good overall yield.
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Doi:10.1016/j.bmc.2019.05.012
(2019)Doi:10.1021/ja01145a020
(1951)Doi:10.1039/c3dt52137k
(2014)Doi:10.1021/ja00077a069
(1993)Doi:10.1021/ja00079a009
(1993)Doi:10.1021/ja00073a057
(1993)
