Tetrahedron Letters p. 4111 - 4114 (1994)
Update date:2022-09-26
Topics:
Taniguchi, Yuki
Nakahashi, Manabu
Kuno, Tatsuhiro
Tsuno, Masumi
Makioka, Yoshikazu
Takaki, Ken
Fujiwara, Yuzo
Ytterbium metal reacts with trimethylsilyl bromide (TMS-Br) to give divalent YbBr2. YbBr2 thus formed in situ, causes coupling reactions of aliphatic ketones and α,β-unsaturated ketones to give bissilylated 1,2-diols and 1,6-ketones, respectively, in good yields.
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