Tetrahedron Asymmetry p. 2007 - 2016 (1996)
Update date:2022-08-03
Topics:
Brimble, Margaret A.
Heathcock, Clayton H.
Nobin, Gregory N.
The preparation of di-(-)-menthyl diazendicarboxylate 3 is described. Reaction of hydrazine with excess (-)-menthyl chloroformate 1 afforded dimenthyl diazanedicarboxylate 2 which was then oxidized to the azo-enophile 3. The azo-ene reactions of 3 with th
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