Synthesis and ene reactions of di-(-)-methyl diazenedicarboxylate

DOI: 10.1016/0957-4166(96)00242-X

Source and publish data:

Tetrahedron Asymmetry p. 2007 - 2016 (1996)

Update date:2022-08-03

Topics:

Authors:

Brimble, Margaret A.

Heathcock, Clayton H.

Nobin, Gregory N.

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Article abstract of DOI:10.1016/0957-4166(96)00242-X

The preparation of di-(-)-menthyl diazendicarboxylate 3 is described. Reaction of hydrazine with excess (-)-menthyl chloroformate 1 afforded dimenthyl diazanedicarboxylate 2 which was then oxidized to the azo-enophile 3. The azo-ene reactions of 3 with th

Full text of DOI:10.1016/0957-4166(96)00242-X

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