Protection of a protecting group: Preparation of stable N-silylated t-butyl carbamates

DOI: 10.1016/S0040-4039(96)02271-X

Source and publish data:

Tetrahedron Letters p. 191 - 194 (1997)

Update date:2022-07-30

Topics:

Authors:

Roby, Johanne

Voyer, Normand

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1016/S0040-4039(96)02271-X

The practical preparation of N-silylated carbamates (typified by 1) is reported. These compounds are synthesized in high yields by treating N-t-Boc-protected primary amines with silyl triflate reagents in dichloromethane in the presence of triethylamine.

Full text of DOI:10.1016/S0040-4039(96)02271-X

Products guided by the article

Product name:N-(triisopropylsilyl)-N-(tert-butyloxycarbonyl)benzylamine

Cas No:186375-61-1

R&D Labs maybe for 186375-61-1

HANGZHOU TOYOND BIOTECH CO., LTD

Contact:+86-571-86965177

Address:No. 189, Fengqi East Road, Hangzhou, China
Wuhan Konberd Biotech Co., Ltd.

Contact:+86-27-87205925

Address:NO.666, Gaoxin Road, Eastlake High-tech zone
Wuhan Konberd Biotech Co., Ltd.

Contact:+86-27-87205925

Address:NO.666, Gaoxin Road, Eastlake High-tech zone
Anhui Qingyun Pharmaceutical and Chemical Co.,Ltd

Contact:+86-551-63633067

Address:Shuangfeng Road Hefei Anhui
FOSHAN NANHAI ZHONGNAN PHARMACEUTICAL FACTORY

Contact:0086-0757-85609331

Address:XIAHENGTIAN INDUSTRIAL ZONE,SHAYONG VILLAGE,LISHUI TOWN

Relevant to this article

Synthesis of substituted dibenzophospholes. Part 9. Preparation of two water-soluble phosphinic-polyphosphonic acids

Doi:10.1039/P19960002889
(1996)
New 2/2-type surfactants via anomeric O-alkylation of mannofuranose

Doi:10.1016/S0008-6215(96)00272-8
(1997)
Model systems for flavoenzyme activity: One- and two-electron reduction of flavins in aprotic hydrophobic environments

Doi:10.1021/ja963704a
(1997)
Synthesis and reactivity of bimetallic iron-rhenium silyl complexes: Crystal structures of [(OC)₃{(MeO)₃Si}Fe(μ-dppm) Re(CO)₄] and [(OC)₃Fe(μ-Br)(μ-dppm)Re(CO)₃]

Doi:10.1016/S0022-328X(96)06524-2
(1996)
Synthesis and anticonvulsant properties of a novel series of 2-substituted amino-5-aryl-1,3,4-oxadiazole derivatives

Doi:10.1002/jhet.5570210538
(1984)
Phosphorated 1,2-oxazabuta-1,3-dienes as synthetic tools for the preparation of a-amino phosphorus derivatives and functionalized nitrogen-containing heterocycles

Doi:10.1080/10426507.2010.522632
(2011)

Article Doi