Tetrahedron Letters p. 5907 - 5910 (1997)
Update date:2022-08-05
Topics:
Parsons, Andrew F.
Pettifer, Robert M.
The cyclisation of amino aldehydes using Bu3SnH in boiling benzene is reported. The reaction proceeds via addition of a tributyltin radical to the aldehyde forming an O-stannyl ketyl and radical cyclisation onto electron poor or rich double bonds gives rise to hydroxy pyrrolidines and piperidines.
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