Tetrahedron Letters p. 183 - 186 (1998)
Update date:2022-08-04
Topics:
Ahmed, Feryan
Forsyth, Craig J.
A convergent synthesis of the C31-C46 domain of the phorboxazole natural products has been developed. This involved the preparation of a C39-C46 dienyl iodide and a C31-C37 aldehyde, followed by their CrCl2-mediated coupling and final installation of the C46 (E)-vinyl bromide via an alkyne hydrostannation-bromination sequence.
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