Tetrahedron Letters p. 1441 - 1444 (2017)
Update date:2022-08-02
Topics:
Mohamadi, Ali
Miller, Lawrence W.
Pre-organized polyaminopolycarboxylate chelators Cy-TTHA and Cy-DTPA were synthesized via modular five-step syntheses from commercially available starting materials in ～62% and 47% overall yields, respectively. Furthermore, strategies are reported for the efficient preparation of mono- and di-reactive, tert-butyl-protected TTHA/Cy-TTHA to selectively functionalize central chelators’ carboxylic acids.
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