Zeitschrift fur Anorganische und Allgemeine Chemie p. 1901 - 1906 (1996)
Update date:2022-08-05
Topics:
Jansen, Martin
Mueller, Ralph
Li2H4I2O10 has been obtained as an intermediate during the dehydration of LiH4IO6 · H2O to LiIO4, for the first time. According to the results of an X-ray structure determination (monoclinic, P21/n, a = 533.98(4), b = 471.85(4), c = 1431.48(10) pm, β = 91.614(7)°, Z = 2, 726 diffractometer data, R = 0.056), Li2H4I2O10 contains the previously unknown tetrahydrogendimesoperiodate ion H4I2O102-, consisting of two edge-shared IO6 octahedra. They are connected with LiO6 octahedra via common edges and vertices. The crystals are non-merohedrally twinned along (100). Johann Ambrosius Barth 1996.
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