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Basic Information
CAS No.: 78628-80-5
Name: Terbinafine hydrochloride
Molecular Structure:
Molecular Structure of 78628-80-5 (Terbinafine hydrochloride)
Formula: C21H26ClN
Molecular Weight: 327.897
Synonyms: Lamisil Krem;Terbinafina [Spanish];Terbinafien HCl;Terbinafine hydrochloride (Lamisil);(E)-N-(6,6-Dimethyl-2-hepten-4-ynyl)-N-methyl-1-naphthalenemethylamine hydrochloride;Terbinafine hydrochloride (JAN);Terbinafinum [Latin];SF 86-327 hydrochloride;(E)-N,6,6-trimethyl-N-(naphthalen-1-ylmethyl)hept-2-en-4-yn-1-amine hydrochloride;Terbinnafine HCL;1-Naphthalenemethanamine, N-(6,6-dimethyl-2-hepten-4-ynyl)-N-methyl-, (E)-, monohydrochloride;Terbinafine HCL(DMF) and its intermediates;Lamisil (TN);Lamisil;N-[(2E)-6,6-dimethyl-2-Hepten-4-yl]-N-methyl-1-naphthalenemethylamine hydrochloride;
EINECS: 245-385-8
Density: 1.007g/cm3
Melting Point: 204-208 °C
Boiling Point: 417.9 °C at 760 mmHg
Flash Point: 183.7 °C
Appearance: Crystalline powder
Hazard Symbols: IrritantXi, DangerousN
Risk Codes: 36/37/38-50/53
Safety: 26-36/37/39-61-60
Transport Information: UN 3077 9/PG 3
PSA: 3.24000
LogP: 5.67930
Synthetic route
14489-75-9

N-methyl-1-naphthalenemethylamine

287471-30-1

1-chloro-6,6-dimethyl-hept-2-ene-4-yn

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
Stage #1: N-methyl-1-naphthalenemethylamine; 1-chloro-6,6-dimethyl-hept-2-ene-4-yn With potassium carbonate In water at 80℃; for 4h; Large scale;
Stage #2: With hydrogenchloride In water at 0 - 10℃; Large scale;
93%
387383-30-4

N-(3-chloroallyl)-1-methyl-1-naphthylmethylamine

917-92-0

2,2-dimethyl-3-butyne

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
Stage #1: N-(3-chloroallyl)-1-methyl-1-naphthylmethylamine; 3,3-Dimethylbut-1-yne With copper(l) iodide; N-butylamine; triphenylphosphine; palladium dichloride at 60 - 65℃; for 20h;
Stage #2: With hydrogenchloride In water at 85 - 90℃; for 0.5h; Temperature;
82.6%
14489-75-9

N-methyl-1-naphthalenemethylamine

78629-20-6

3-hydroxy-6,6-dimethylhept-1-ene-4-yne

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
Stage #1: 3-hydroxy-6,6-dimethylhept-1-ene-4-yne With hydrogenchloride; trichlorophosphate In methanol at 0 - 20℃; for 20 - 24h;
Stage #2: N-methyl-1-naphthalenemethylamine With sodium hydroxide at 80℃;
Stage #3: With hydrogenchloride In dichloromethane; water at 20℃;
81%
91161-71-6

terbinafin

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In water; butanone at 20 - 30℃; for 0.25h;75%
With hydrogenchloride In water; butanone at 0 - 20℃; for 2.5h; Product distribution / selectivity;66.4%
With hydrogenchloride In isopropyl alcohol at 0 - 20℃; for 0.5h; Product distribution / selectivity;63%
2N-hydrochloric acid

2N-hydrochloric acid

556811-68-8

1-(2'-furyl)-2,2-dimethylpropan-1-one tosyl hydrazone

65473-13-4

N-methyl-1-naphthalenemethylamine hydrochloride

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
With sodium hydroxide; sodium borohydrid In ethyl acetate; isopropyl alcohol; toluene50.3%
With sodium hydroxide; sodium borohydrid In ethanol; ethyl acetate; toluene45.5%
With sodium hydroxide; sodium borohydrid In ethyl acetate; toluene; tert-butyl alcohol19%
2N-hydrochloric acid

2N-hydrochloric acid

2N-hydrochloride acid

2N-hydrochloride acid

556811-67-7

1-(2'-furyl)-2,2-dimethylpropan-1-one benzenesulfonyl hydrazone

65473-13-4

N-methyl-1-naphthalenemethylamine hydrochloride

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
With sodium hydroxide; sodium borohydrid In ethyl acetate; isopropyl alcohol; toluene18.6%
2N-hydrochloric acid

2N-hydrochloric acid

65473-13-4

N-methyl-1-naphthalenemethylamine hydrochloride

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
With sodium hydroxide; sodium borohydrid; acetic acid In ethyl acetate; toluene; tert-butyl alcohol17.4%
2N-hydrochloric acid

2N-hydrochloric acid

2N-hydrochloride acid

2N-hydrochloride acid

556811-69-9

1-(2'-furyl)-2,2-dimethylpropan-1-one 4-methoxybenzenesulfonyl hydrazone

65473-13-4

N-methyl-1-naphthalenemethylamine hydrochloride

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
With sodium hydroxide; sodium borohydrid In ethyl acetate; isopropyl alcohol; toluene11.7%
2N-hydrochloric acid

2N-hydrochloric acid

2N-hydrochloride acid

2N-hydrochloride acid

556811-66-6

1-(2'-furyl)-2,2-dimethylpropan-1-one methanesulfonyl hydrazone

65473-13-4

N-methyl-1-naphthalenemethylamine hydrochloride

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
With sodium hydroxide; sodium borohydrid In ethyl acetate; isopropyl alcohol; toluene10.9%
2N-hydrochloric acid

2N-hydrochloric acid

2N-hydrochloride acid

2N-hydrochloride acid

556811-68-8

1-(2'-furyl)-2,2-dimethylpropan-1-one tosyl hydrazone

65473-13-4

N-methyl-1-naphthalenemethylamine hydrochloride

78628-80-5

terbinafine hydrochloride

Conditions
ConditionsYield
With sodium hydroxide; sodium borohydrid In methanol; ethyl acetate; toluene10.4%
Downstream Products
91161-71-6
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    78628-80-5 - Physico-chemical Properties Molecular Formula C21H26ClN Molar Mass 327.89 Density 1.007g/cm3 Melting Point 204-208°C Boling Point 417.9°C at 760 mmHg Flash Poi

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  • Terbinafine Hydrochloride	CAS:78628-80-5

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    Terbinafine Hydrochloride CAS:78628-80-5

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    Product Name: Terbinafine Purity: 98%min Appearance: White crystalline powder CAS No.: 91161-71-6 Molecular formula: C21H25N Molecular weight: 291.43000 Appearance: White Powder Storage:Store in cool and dry place, away from sun ligh

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    MSDS/COA Download

    Terbinafine Hydrochloride USDMF EDMF

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Specification

1. Introduction of Terbinafine hydrochloride

Terbinafine hydrochloride, with the IUPAC Name of (E)-N,6,6-Trimethyl-N-(naphthalen-1-ylmethyl)hept-2-en-4-yn-1-amine hydrochloride, has the Classification Code which include Antifungal; Drug / Therapeutic Agent; Human Data; Reproductive Effect. And this chemical belongs to the Product Categories which include Antifungal; APIs; Acetylenes; Antifungals for Research and Experimental Use; Biochemistry; Functionalized Acetylenes; Amines; Aromatics; Intermediates & Fine Chemicals; Pharmaceuticals; Terbinafine.

2. Properties of Terbinafine hydrochloride

Terbinafine hydrochloride has the following properties: (1)H bond acceptors: 1; (2)Freely Rotating Bonds: 5; (3)Polar Surface Area: 3.24; (4)Flash Point: 183.7 °C; (5)Enthalpy of Vaporization: 67.13 kJ/mol; (6)Boiling Point: 417.9 °C at 760 mmHg; (7)Vapour Pressure: 3.42E-07 mmHg at 25°C.

3. Toxicity of Terbinafine hydrochloride

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 subcutaneous > 2gm/kg (2000mg/kg) SENSE ORGANS AND SPECIAL SENSES: PTOSIS: EYE

BEHAVIORAL: ATAXIA

BLOOD: CHANGES IN SPLEEN
Kiso to Rinsho. Clinical Report. Vol. 24, Pg. 7888, 1990.
rat LD50 skin > 2gm/kg (2000mg/kg) SENSE ORGANS AND SPECIAL SENSES: PTOSIS: EYE

BEHAVIORAL: ATAXIA

BLOOD: CHANGES IN SPLEEN
Kiso to Rinsho. Clinical Report. Vol. 24, Pg. 7922, 1990.
rat LD50 subcutaneous > 2gm/kg (2000mg/kg) SENSE ORGANS AND SPECIAL SENSES: PTOSIS: EYE

BLOOD: CHANGES IN SPLEEN

BEHAVIORAL: ATAXIA
Kiso to Rinsho. Clinical Report. Vol. 24, Pg. 7922, 1990.
women TDLo oral 210mg/kg/6W-I (210mg/kg) SENSE ORGANS AND SPECIAL SENSES: CHANGE IN FUNCTION: TASTE Lancet. Vol. 339, Pg. 1483, 1992.

4. Safety Information of Terbinafine hydrochloride

Hazard Codes of Terbinafine Hcl (CAS NO.78628-80-5): IrritantXi,DangerousN
Risk Statements: 36/37/38-50/53 
R36/37/38: Irritating to eyes, respiratory system and skin. 
R50/53: Very toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment.
Safety Statements: 26-36/37/39-61-60 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection. 
S61: Avoid release to the environment. Refer to special instructions / safety data sheets. 
S60: This material and its container must be disposed of as hazardous waste.
RIDADR: UN 3077 9/PG 3 
 
5. Use and Preparation of Terbinafine hydrochloride

Terbinafine Hcl is a synthetic allylamine antifungal. Its nature is highly lipophilic, easily accumulate in the skin, nails, and fat tissue. Terbinafine Hcl is orally active, antimycotic allylamine related to naftifine.It's a specfic inhibitor of squalene epoxidase,and also a key enzyme in fungal Ergosterol biosynthesis.