Tetrahedron Letters p. 9271 - 9274 (1998)
Update date:2022-08-03
Topics: Yield Solvent Work-Up Reaction Conditions Convenient route Experimental Terms Polyhydroxyalkyl-heterocycles Cerium (IV)
Moreno-Vargas, Antonio J.
Robina, Inmaculada
Fernandez-Bolanos, Jose G.
Fuentes, Jose
The synthesis of 3-ethoxycarbonyl-2,5-diformylpyrrole (2) from 3- ethoxycarbonyl-2-methyl-5-D-(arabino-tetritol-l-yl)pyrrole (1) by oxidation with ceric ammonium nitrate is described. When the reaction was applied to related furan derivatives, ethyl (5S,6R,7R)-2-acetyl-5,6,7,8- tetrabenzyloxyoct-2-enoate (8) was obtained as an E/Z mixture.
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Doi:10.1039/a806283h
(1998)Doi:10.1016/S0022-1139(98)00247-4
(1998)Doi:10.1016/S0040-4039(98)02162-5
(1998)Doi:10.3987/COM-98-S31
(1998)Doi:10.1021/jo981538e
(1999)Doi:10.1016/S0040-4039(98)02274-6
(1999)
