New masked δ-lithiocarbonyl compounds: Preparation and synthetic applications

DOI: 10.1016/S0040-4020(01)80409-9

Source and publish data:

Tetrahedron p. 4923 - 4938 (1993)

Update date:2022-08-02

Topics:

Authors:

Gil, Juan F.

Ramon, Diego J.

Yus, Miguel

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Article abstract of DOI:10.1016/S0040-4020(01)80409-9

The reaction of 2-(4-chlorobutyl)-1,3-dioxolanes (1a-c) or 2-(4-chlorobutyl)-2-ethyl-1,3-dithiane (1d) with an excess of lithium powder and a catalytic amount of naphthalene (8 mol %) in THF at - 78°C leads to a solution of the corresponding masked lithiu

Full text of DOI:10.1016/S0040-4020(01)80409-9

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