Tetrahedron p. 4923 - 4938 (1993)
Update date:2022-08-02
Topics:
Gil, Juan F.
Ramon, Diego J.
Yus, Miguel
The reaction of 2-(4-chlorobutyl)-1,3-dioxolanes (1a-c) or 2-(4-chlorobutyl)-2-ethyl-1,3-dithiane (1d) with an excess of lithium powder and a catalytic amount of naphthalene (8 mol %) in THF at - 78°C leads to a solution of the corresponding masked lithiu
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