Synthesis of deuterium labelled acids

DOI: 10.1002/(SICI)1099-1344(199909)42:9<835::AID-JLCR244>3.0.CO;2-R

Source and publish data:

Journal of labelled compounds and radiopharmaceuticals p. 835 - 842 (1999)

Update date:2022-07-30

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Authors:

Kadam Kadam

Desai Desai

Mane Mane

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Article abstract of DOI:10.1002/(SICI)1099-1344(199909)42:9<835::AID-JLCR244>3.0.CO;2-R

Knoevenagel condensation of Meldrum's acid (1) with benzaldehyde, anisaldehyde, furfural, cinnamaldehyde and acetone gave the corresponding alkylidene derivatives (3) which were reduced with sodium borohydride to yield alkyl Meldrum's acids (4). Reaction

Full text of DOI:10.1002/(SICI)1099-1344(199909)42:9<835::AID-JLCR244>3.0.CO;2-R

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Product name:β-monodeuterated 4-methoxybenzyl Meldrum's acid

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