Bulletin of the Chemical Society of Japan p. 3716 - 3718 (1990)
Update date:2022-08-04
Topics: Silyl enol ethers α,β-Unsaturated Ketones Novel Synthesis Acetals convenient synthesis Tin(II) chloride Organic halide
Oriyama, Takeshi
Iwanami, Katsuyuki
Miyauchi,Yuka
Koga, Gen
Acetals react with silyl enol ethers to give condensation products in good yield by the action of a reactive halide such as acetyl chloride or methoxymethyl chloride along with a catalytic amount of SnCl2.The procedure employing excessive amount of halide offers a novel and convenient method to synthesize conjugated enones.
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