Journal of Organometallic Chemistry p. 173 - 183 (1992)
Update date:2022-08-03
Topics:
Ozawa, Fumiyuki
Chikaoka, Satoyuki
Cao, Xi-Zhang
Yamamoto, Akio
Treatment of Ru(COEt)Cl(CO)(PPh3)2 (1) with secondary amines (R2NH) under pressure of CO and/or ethylene gives propionyl-carbamoyl complexes Ru(COEt)(CONR2)(CO)(PPh3)2 (NR2 = NEt2 (4a), N(CH2)4CH2 (4b), NMe2 (4c)) together with the ammonium salt R2NH2Cl.Complexes 4a-c have been isolated as pale yellow crystals and characterized by means of NMR and IR spectroscopy and elemental analysis.Reactions of Fe(COMe)I(CO)2(PMe3)2 and
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