Advanced Synthesis and Catalysis p. 1164 - 1172 (2016)
Update date:2022-08-05
Topics:
Bergami, Matteo
Protti, Stefano
Ravelli, Davide
Fagnoni, Maurizio
A convenient photochemical flow protocol for the formation of aryl-carbon bonds via photogenerated phenyl cations has been developed. A wide range of phenylated products, including biaryls, allylarenes, 2-arylacetals and benzyl γ-lactones, was smoothly synthesized in satisfactory yields under metal-free conditions. The adoption of a flow reactor often allowed us to adopt higher concentrations of substrates and shorter irradiation times compared to those usually employed in batch systems.
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