Tetrahedron Letters p. 2737 - 2740 (1987)
Update date:2022-07-30
Topics:
Minami, Ichiro
Yuhara, Masami
Tsuji, Jiro
As a new protective group of amines, 1-isopropylallyloxycarbonyl (IPAoc) group was developed.IPAoc group can be removed by treatment with a palladium-phosphine catalyst forming carbon dioxide and 4-methyl-1,3-pentadiene by the decarboxylation and β-hydrogen elimination of (?-1-isopropylallyl)-palladium intermediate under neutral condititons.The present protection-deprotection was applied to a one-pot peptide synthesis.
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(1962)
