Journal of the Chemical Society. Chemical communications p. 1095 - 1096 (1984)
Update date:2022-08-04
Topics:
Baldwin, Jack E.
Adlington, Robert M.
Bottaro, Jeffrey C.
Jain, Ashok U.
Kolhe, Jayant N.
et al.
The lithium salts of t-butyl- and trityl-hydrazones react with methyl crotonate to form C-trapped azo-esters and similar products were observed from a thermal ene-reaction of aldehyde t-butylhydrazones with methyl acrylate or acrylonitrile, and aldehyde phenylhydrazones with methyl acrylate; these products can be diverted into synthetically useful γ-keto-esters, γ-keto-nitriles, saturated esters, γ-alkyl-2-pyrrrolidones, and γ-amino-esters.
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Doi:10.1246/bcsj.65.620
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