Journal of Organic Chemistry p. 2547 - 2548 (1980)
Update date:2022-08-05
Topics:
Kawada, Yuzo
Iwamura, Hiizu
The title compound was prepared by the thermolysis in perfluorodecalin of 1-triptycyl 1-triptyceneperoxycarboxylate which in turn was obtained by the reaction of 1-triptycyllithium with oxygen followed by treatment with 1-triptycenecarbonyl chloride.No sign of restricted rotation around the bridgehead-to-oxygen bonds of the ether was indicated by the 1H and 13C NMR spectra in spite of its overcrowded molecular framework.
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Doi:10.1016/0022-328X(85)80095-4
(1985)Doi:10.1016/S0022-1139(00)82577-4
(1980)Doi:10.1002/hlca.19800630213
(1980)Doi:10.1016/S0022-328X(00)81794-5
(1980)Doi:10.1021/ja01105a016
(1953)Doi:10.1271/bbb1961.44.427
(1980)
