1-Iodo-polyfluoroalkanes from polyfluoroalkoxy trimethylsilanes and iodochloro triphenylphosphorane

DOI: 10.1016/S0040-4039(00)73201-1

Source and publish data:

Tetrahedron Letters p. 1941 - 1944 (1994)

Update date:2022-08-02

Topics:

Authors:

Montanari

Quici Quici

Resnati Resnati

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Article abstract of DOI:10.1016/S0040-4039(00)73201-1

Polyfluoroalkoxy trimethylsilanes R(f)CH₂OSi(CH₃)₃ (from the alcohols R(f)CH₂OH and HMDS), react with Pb₃PICI (from ICI and Ph₃P) eliminating (CH₃)₃SiCl. Pyrolysis of the residues gives Ph₃PO and pure iodides R(f)CH₂I.

Full text of DOI:10.1016/S0040-4039(00)73201-1

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