Journal of Organic Chemistry p. 3090 - 3094 (1982)
Update date:2022-08-02
Topics:
Shono, Tatsuyo
Matsumura, Yoshihiro
Tsubata, Kenji
Sugihara, Yoshihiro
Electroorganic synthesis of cyclopropanes from dimethanesulfonates of 1,3-diols is described.The process involves reduction of 1,3-dicarbonyl compounds with LiAlH followed by esterification with methanesulfonyl chloride and electroreduction.
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