Tetrahedron Letters p. 1431 - 1434 (1987)
Update date:2022-09-26
Topics:
Kita, Yasuyuki
Itoh, Fumio
Tamura, Osamu
Ke, Ya Yuan
Tamura, Yasumitsu
N-Benzoyl L-daunosamine was synthesized with high stereoselectivity utilizing a 1,3-addition of ketene silyl acetal (3a) to the chiral nitrone, (Z)-((4R)-trans-2,2,5-trimethyl-1,3-dioxolan-4-yl)methylene((1S)-1-phenylethyl)amine N-oxide (4c) accompanied by a silyl group-transfer in acetonitrile under mild conditions.
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