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Meglumine 6284-40-8
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USD $ 38.0-38.0 / Kilogram 25 Kilogram 2000 Kilogram/Week ShangHai Soyoung Biotechnology Inc Contact Supplier
Methylglucamine
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High quality n-methylglucamine
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N-Methyl-D-glucamine
Cas No: 6284-40-8
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6284-40-8 Usage

Purification Methods

Crystallise N-methyl-D(-)-glucamine from MeOH. Its solubility in H2O is 10%. [Karrer & Herkenrath Helv Chim Acta 20 83 1957 also for other N-alkyl derivatives, Beilstein 4 IV 1914.]

Pharmaceutical Applications

Meglumine is an organic base used as a pH-adjusting agent and solubilizing agent, primarily in the preparation of soluble salts of iodinated organic acids used as X-ray contrast media.

Production Methods

Meglumine is prepared by the imination of glucose and monomethylamine, in an alcoholic solution, followed by catalytic hydrogenation.

Chemical Properties

white to almost white crystalline powder

Uses

antiinflammatory

storage

Meglumine does not polymerize or dehydrate unless heated above 150°C for prolonged periods. The bulk material should be stored in a well-closed container in a cool, dry place. Meglumine should not be stored in aluminum containers since it reacts to evolve hydrogen gas; it discolors if stored in containers made from copper or copper alloys. Stainless steel containers are recommended.

Chemical Properties

Meglumine occurs as a white to slightly yellow-colored crystalline powder; it is odorless or with a slight odor.

Safety

Meglumine is widely used in parenteral pharmaceutical formulations and is generally regarded as a nontoxic material at the levels usually employed as an excipient. LD50 (mouse, IP): 1.68 g/kg

Brand name

Renovue (Bracco).

Uses

excipient in cosmetics and X-ray contrast media

Regulatory Status

Included in the FDA Inactive Ingredients Database (injections; oral tablets). Included in parenteral medicines licensed in the UK.

Definition

ChEBI: A hexosamine that is D-glucitol in which the hydroxy group at position 1 is substituted by the nitrogen of a methylamino group. A crystalline base, it is used in preparing salts of certain acids for use as diagnostic radiopaque media, whi e its antimonate is used as an antiprotozoal in the treatment of leishmaniasis.

Incompatibilities

Incompatible with aluminum, copper, mineral acids, and oxidizing materials. Differential scanning calorimetry studies suggest meglumine is incompatible with glipizide.
InChI:InChI=1/C7H17NO5/c1-8-2-4(10)6(12)7(13)5(11)3-9/h4-13H,2-3H2,1H3/p+1/t4-,5-,6+,7-/m1/s1

6284-40-8 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (L14282)  N-Methyl-D-glucamine, 99%    6284-40-8 50g 101.0CNY Detail
Alfa Aesar (L14282)  N-Methyl-D-glucamine, 99%    6284-40-8 250g 282.0CNY Detail
Sigma-Aldrich (PHR1324)  Meglumine  pharmaceutical secondary standard; traceable to USP and PhEur 6284-40-8 PHR1324-1G 718.73CNY Detail
Sigma-Aldrich (Y0001209)  N-Methyl-D-glucamine  European Pharmacopoeia (EP) Reference Standard 6284-40-8 Y0001209 1,880.19CNY Detail
USP (1379140)  Meglumine  United States Pharmacopeia (USP) Reference Standard 6284-40-8 1379140-500MG 4,326.66CNY Detail
Sigma (M2004)  N-Methyl-D-glucamine  99.0-100.5% (titration) 6284-40-8 M2004-100G 223.47CNY Detail
Sigma (M2004)  N-Methyl-D-glucamine  99.0-100.5% (titration) 6284-40-8 M2004-500G 671.58CNY Detail
Sigma (M2004)  N-Methyl-D-glucamine  99.0-100.5% (titration) 6284-40-8 M2004-1KG 1,263.60CNY Detail
Sigma-Aldrich (66930)  N-Methyl-D-glucamine  ReagentPlus®, ≥99.0% (T) 6284-40-8 66930-100G 403.65CNY Detail
Sigma-Aldrich (66930)  N-Methyl-D-glucamine  ReagentPlus®, ≥99.0% (T) 6284-40-8 66930-500G 1,166.49CNY Detail

6284-40-8SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name N-methylglucamine

1.2 Other means of identification

Product number -
Other names N-Methyl-D-glucamine

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:6284-40-8 SDS

6284-40-8Synthetic route

N-methyl-D-gluconamide
24758-59-6

N-methyl-D-gluconamide

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

Conditions
ConditionsYield
With ammonia borane; palladium/alumina at 78℃; under 975.098 - 48004.8 Torr; for 2h; Temperature; Pressure; Reagent/catalyst; Inert atmosphere; Large scale;69.3%
D-glucose
50-99-7

D-glucose

methylamine
74-89-5

methylamine

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

Conditions
ConditionsYield
With hydrogen In water at 10 - 100℃; under 5171.62 - 25858.1 Torr; for 21.5h;62.5%
With nickel kieselguhr; water at 95 - 120℃; under 36775.4 - 102971 Torr; Hydrogenation;
With ethanol Hydrierung des Reaktionsprodukts an Palladium-Kohle in Methanol bei 60grad/20-25at;
D-glucose
50-99-7

D-glucose

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

Conditions
ConditionsYield
With methylamine
D-glucose
50-99-7

D-glucose

methylaminomethanol
3400-38-2

methylaminomethanol

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

magnesium stearate
557-04-0

magnesium stearate

A

poloxamer

poloxamer

B

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

D-glucose
50-99-7

D-glucose

methylamine
74-89-5

methylamine

A

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

B

N,N`-dimethylethylenediamine
110-70-3

N,N`-dimethylethylenediamine

Conditions
ConditionsYield
With 5 wt% ruthenium/carbon; hydrogen In water at 124.84℃; under 56255.6 Torr; for 1h;
5-({4-[(4-butylphenyl)ethynyl]benzyl}{[2-(ethoxycarbonyl)cyclopropyl]methyl}amino)-2-fluorobenzoic acid

5-({4-[(4-butylphenyl)ethynyl]benzyl}{[2-(ethoxycarbonyl)cyclopropyl]methyl}amino)-2-fluorobenzoic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

5-({4-[(4-butylphenyl)ethynyl]benzyl}{[2-(ethoxycarbonyl)cyclopropyl]methyl}amino)-2-fluorobenzoic acid N-methyl-D-glucamine salt

5-({4-[(4-butylphenyl)ethynyl]benzyl}{[2-(ethoxycarbonyl)cyclopropyl]methyl}amino)-2-fluorobenzoic acid N-methyl-D-glucamine salt

Conditions
ConditionsYield
In methanol; water100%
gadolinium(III) oxide

gadolinium(III) oxide

2-[1,4,7,10-tetraaza-4,7-di(1-carboxy-2-benzyloxy-ethyl)-10-carboxymethyl-cyclododecane-1-yl]-3-benzyloxypropionic acid
124628-06-4

2-[1,4,7,10-tetraaza-4,7-di(1-carboxy-2-benzyloxy-ethyl)-10-carboxymethyl-cyclododecane-1-yl]-3-benzyloxypropionic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

{gadolinium(C8H17N4(CH2COO)(CH(COO)CH2OCH2C6H5)3)(D(-)-N-methylglucamine)}

{gadolinium(C8H17N4(CH2COO)(CH(COO)CH2OCH2C6H5)3)(D(-)-N-methylglucamine)}

Conditions
ConditionsYield
In water heating to 70°C until a clear soln. was obtained; evapn. (vac.) and isolation after drying to const. weight; elem. anal.;100%
gadolinium(III) oxide

gadolinium(III) oxide

2-[1,4,7,10-tetraaza-4-(1-carboxy-2-benzyloxy-ethyl)-7,10-di(carboxymethyl)-cyclododecane-1-yl]-3-benzyloxypropionic acid
124628-02-0

2-[1,4,7,10-tetraaza-4-(1-carboxy-2-benzyloxy-ethyl)-7,10-di(carboxymethyl)-cyclododecane-1-yl]-3-benzyloxypropionic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

{gadolinium(C8H17N4(CH2COO)2(CH(COO)CH2OCH2C6H5)2)(D(-)-N-methylglucamine)}

{gadolinium(C8H17N4(CH2COO)2(CH(COO)CH2OCH2C6H5)2)(D(-)-N-methylglucamine)}

Conditions
ConditionsYield
In water heating to 70°C until a clear soln. was obtained; evapn. (vac.) and isolation after drying to const. weight; elem. anal.;100%
gadolinium(III) oxide

gadolinium(III) oxide

2-[1,4,7,10-tetraaza-4,7,10-tri(carboxymethyl)-cyclododecane-1-yl]-3-benzyloxypropionic acid
124628-08-6

2-[1,4,7,10-tetraaza-4,7,10-tri(carboxymethyl)-cyclododecane-1-yl]-3-benzyloxypropionic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

{gadolinium(C8H17N4(CH2COO)3CH(COO)CH2OCH2C6H5)(D(-)-N-methylglucamine)}

{gadolinium(C8H17N4(CH2COO)3CH(COO)CH2OCH2C6H5)(D(-)-N-methylglucamine)}

Conditions
ConditionsYield
In water heating to 70°C until a clear soln. was obtained; evapn. (vac.) and isolation after drying to const. weight; elem. anal.;100%
gadolinium(III) oxide

gadolinium(III) oxide

2-[1,4,7,10-tetraaza-7-(1-carboxy-2-benzyloxy-ethyl)-4,10-di(carboxymethyl)-cyclododecane-1-yl]-3-benzyloxypropionic acid
124628-04-2

2-[1,4,7,10-tetraaza-7-(1-carboxy-2-benzyloxy-ethyl)-4,10-di(carboxymethyl)-cyclododecane-1-yl]-3-benzyloxypropionic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

{gadolinium(C8H17N4(CH2COO)2(CH(COO)CH2OCH2C6H5)2)(D(-)-N-methylglucamine)}

{gadolinium(C8H17N4(CH2COO)2(CH(COO)CH2OCH2C6H5)2)(D(-)-N-methylglucamine)}

Conditions
ConditionsYield
In water heating to 70°C until a clear soln. was obtained; evapn. (vac.) and isolation after drying to const. weight; elem. anal.;100%
D-isoglutamyl-D-tryptophan
186087-26-3

D-isoglutamyl-D-tryptophan

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

D-isoglutamyl-D-tryptophan mono-N-methyl-D-glucamine salt
1034125-74-0

D-isoglutamyl-D-tryptophan mono-N-methyl-D-glucamine salt

Conditions
ConditionsYield
In water at 20℃; pH=~ 7;100%
In water at 20℃; for 168h; pH=Ca. 7;100%
5-chloro-2-([(2-([3-(furan-3-yl)phenyl]amino)-2-oxoehtoxy)acetyl]amino)benzoic acid
1190221-43-2

5-chloro-2-([(2-([3-(furan-3-yl)phenyl]amino)-2-oxoehtoxy)acetyl]amino)benzoic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

5-chloro-2-([(2-([3-(furan-3-yl)phenyl]amino)-2-oxoethoxy)acethyl]amino)benzoic acid N-methyl-D-glucaminesalt
1190221-63-6

5-chloro-2-([(2-([3-(furan-3-yl)phenyl]amino)-2-oxoethoxy)acethyl]amino)benzoic acid N-methyl-D-glucaminesalt

Conditions
ConditionsYield
In methanol for 0.5h;100%
(S)-2-((5Z,8Z,11Z,14Z,17Z)-icosa-5,8,11,14,17-pentaenamido)-4-methylpentanoic acid

(S)-2-((5Z,8Z,11Z,14Z,17Z)-icosa-5,8,11,14,17-pentaenamido)-4-methylpentanoic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

C7H17NO5*C26H41NO3

C7H17NO5*C26H41NO3

Conditions
ConditionsYield
In methanol at 20℃; for 2h;100%
O-[1-(propofol-O-yl)]cyclobut-1-yl-monoester phosphoric acid

O-[1-(propofol-O-yl)]cyclobut-1-yl-monoester phosphoric acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

O-[1-(propofol-O-yl)]cyclobut-1-yl-monoester dimeglumine phosphate

O-[1-(propofol-O-yl)]cyclobut-1-yl-monoester dimeglumine phosphate

Conditions
ConditionsYield
In water at 20℃; for 1h;100%
1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

epichlorohydrin
106-89-8

epichlorohydrin

C10H22ClNO6

C10H22ClNO6

Conditions
ConditionsYield
In methanol at 20℃; for 72h;100%
2-(5-nitrothiazol-2-yl-carbamoyl)phenyl dihydrogen phosphate

2-(5-nitrothiazol-2-yl-carbamoyl)phenyl dihydrogen phosphate

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

2-(5-nitrothiazol-2-ylcarbamoyl)phenyl dihydrogen phosphate methylglucamine salt

2-(5-nitrothiazol-2-ylcarbamoyl)phenyl dihydrogen phosphate methylglucamine salt

Conditions
ConditionsYield
In methanol at 20℃; for 0.333333h;100%
(4S)-4-[5-(2,5-dichloro-4-[[(4R)-4-[(4-cyclopropyl-1,2,3,4-tetrahydroquinoxalin-1-yl)carbonyl]-1,3-thiazolidin-3-yl]methyl]phenyl)pentanamido]-5-methoxy-5-oxopentanoic acid

(4S)-4-[5-(2,5-dichloro-4-[[(4R)-4-[(4-cyclopropyl-1,2,3,4-tetrahydroquinoxalin-1-yl)carbonyl]-1,3-thiazolidin-3-yl]methyl]phenyl)pentanamido]-5-methoxy-5-oxopentanoic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

methyl (2S)-2-[5-(2,5-dichloro-4-[[(4R)-4-[(4-cyclopropyl-1,2,3,4-tetrahydroquinoxalin-1-yl)carbonyl]-1,3-thiazolidin-3-yl]methyl]phenyl)pentanamido]-4-[methyl[(2S,3R,4R,5R)-2,3,4,5,6-pentahydroxyhexyl]carbamoyl]butanoate

methyl (2S)-2-[5-(2,5-dichloro-4-[[(4R)-4-[(4-cyclopropyl-1,2,3,4-tetrahydroquinoxalin-1-yl)carbonyl]-1,3-thiazolidin-3-yl]methyl]phenyl)pentanamido]-4-[methyl[(2S,3R,4R,5R)-2,3,4,5,6-pentahydroxyhexyl]carbamoyl]butanoate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃;100%
3,8-bis(1-methoxyethyl)deuteroporphyrin IX

3,8-bis(1-methoxyethyl)deuteroporphyrin IX

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

3,8-bis(1-methoxyethyl)porphyrin IX dimeglumine salt

3,8-bis(1-methoxyethyl)porphyrin IX dimeglumine salt

Conditions
ConditionsYield
In ethanol for 1h; Reflux;100%
(R)-3-(4-(2-(2-methyltetrazol-5-yl)pyridine-5-yl)-3-fluorophenyl)-5-hydroxymethyl oxazolidin-2-one dihydrogen phosphate

(R)-3-(4-(2-(2-methyltetrazol-5-yl)pyridine-5-yl)-3-fluorophenyl)-5-hydroxymethyl oxazolidin-2-one dihydrogen phosphate

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

tedizolid phosphate dimeglumine

tedizolid phosphate dimeglumine

Conditions
ConditionsYield
In water at 20℃; Concentration;99.5%
gadolinium(III) oxide

gadolinium(III) oxide

(3β,5β,7α,12α)-3-[[[[[bis[2-[bis(carboxymethyl)amino]ethyl]amino]-acetyl]amino]-acetyl]amino]-7,12-dihydroxycholan-24-oic acid
174267-98-2

(3β,5β,7α,12α)-3-[[[[[bis[2-[bis(carboxymethyl)amino]ethyl]amino]-acetyl]amino]-acetyl]amino]-7,12-dihydroxycholan-24-oic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

gadolinium complex of (3β,5β,7α, 12α)-3-[[[[[bis[2-[bis(carboxymethyl)amino]ethyl]amino]acetyl]amino]acetyl]amino]-7,12-dihydroxycholan-24-oic acid salified with 1-deoxy-1-(methylamino)-D-glucitol (1:2)

gadolinium complex of (3β,5β,7α, 12α)-3-[[[[[bis[2-[bis(carboxymethyl)amino]ethyl]amino]acetyl]amino]acetyl]amino]-7,12-dihydroxycholan-24-oic acid salified with 1-deoxy-1-(methylamino)-D-glucitol (1:2)

Conditions
ConditionsYield
In water at 50℃; for 25h; pH=5.0 - 6.8;99%
2,5-dihydroxy-1,4-dithiane-2,5-dicarboxylic acid
80003-64-1

2,5-dihydroxy-1,4-dithiane-2,5-dicarboxylic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

2,5-dihydroxy-1,4-dithiane-2,5-dicarboxylic acid, bis-((2R,3R,4R,5S)-6-methylaminohexane-1,2,3,4,5-pentol) salt

2,5-dihydroxy-1,4-dithiane-2,5-dicarboxylic acid, bis-((2R,3R,4R,5S)-6-methylaminohexane-1,2,3,4,5-pentol) salt

Conditions
ConditionsYield
In water at 20℃; for 0.166667h;99%
26-succinate-22-deacetyl-neoboutomellerone
1256465-11-8

26-succinate-22-deacetyl-neoboutomellerone

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

26-succinate-22-deacetyl-neoboutomellerone N-methyl-D-glucamine salt
1256465-12-9

26-succinate-22-deacetyl-neoboutomellerone N-methyl-D-glucamine salt

Conditions
ConditionsYield
In ethanol; water for 0.166667h;99%
In ethanol; water for 0.166667h;99%
2,5-dioxopyrrolidin-1-yl pent-4-ynoate
132178-37-1

2,5-dioxopyrrolidin-1-yl pent-4-ynoate

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

N-methyl-N-(4-pentynoyl)-D-glucamine
1448147-88-3

N-methyl-N-(4-pentynoyl)-D-glucamine

Conditions
ConditionsYield
With triethylamine In pyridine; N,N-dimethyl-formamide at 20℃; for 1h;99%
methacryloyl anhydride
760-93-0

methacryloyl anhydride

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

N-methacryloyl-N-methyl-1-amino-1-deoxy-D-glucitol

N-methacryloyl-N-methyl-1-amino-1-deoxy-D-glucitol

Conditions
ConditionsYield
In methanol at 15 - 25℃; for 2h; Solvent;99%
1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

3-(triethoxypropyl) isocyanate
24801-88-5

3-(triethoxypropyl) isocyanate

N-methyl-N-(2,3,4,5,6-pentahydroxyhexyl)-N'-(3-triethoxysilylpropyl)urea

N-methyl-N-(2,3,4,5,6-pentahydroxyhexyl)-N'-(3-triethoxysilylpropyl)urea

Conditions
ConditionsYield
In tetrahydrofuran at 80 - 90℃; for 2.5h;99%
1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

tris(4-hydroxyphenyl)methane triglycidyl ether

tris(4-hydroxyphenyl)methane triglycidyl ether

4,4',4''-tris{2-hydroxy-3-[N-methyl-(2',3',4',5',6'-pentahydroxy-D-gluco-hexyl)amino]propoxy}triphenylmethane

4,4',4''-tris{2-hydroxy-3-[N-methyl-(2',3',4',5',6'-pentahydroxy-D-gluco-hexyl)amino]propoxy}triphenylmethane

Conditions
ConditionsYield
In ethanol for 7h; Reflux;99%
(R)-3-methyl-6-(2-((5-methyl-2-(6-(trifluoromethyl)pyridin-3-yl)-1H-imidazol-1-yl)methyl)phenoxy)hexanoic acid

(R)-3-methyl-6-(2-((5-methyl-2-(6-(trifluoromethyl)pyridin-3-yl)-1H-imidazol-1-yl)methyl)phenoxy)hexanoic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

C24H26F3N3O3*C7H17NO5

C24H26F3N3O3*C7H17NO5

Conditions
ConditionsYield
In tetrahydrofuran; water at 20℃; for 16h; Solvent; Temperature;98.95%
In isopropyl alcohol at 25 - 50℃; for 1.33333h; Solvent; Sealed tube;
In isopropyl alcohol at 25 - 50℃; for 1.33333h; Solvent; Sealed tube; Sonication;
(R)-3-(4-(2-(2-methyltetrazol-5-yl)pyridine-5-yl)-3-fluorophenyl)-5-hydroxymethyl oxazolidin-2-one dihydrogen phosphate

(R)-3-(4-(2-(2-methyltetrazol-5-yl)pyridine-5-yl)-3-fluorophenyl)-5-hydroxymethyl oxazolidin-2-one dihydrogen phosphate

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

tedizolid phosphate monomeglumine

tedizolid phosphate monomeglumine

Conditions
ConditionsYield
In water at 20℃; Concentration;98.9%
1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

wortmannin
19545-26-7

wortmannin

WmC20-N-methyl-glucamine

WmC20-N-methyl-glucamine

Conditions
ConditionsYield
In dimethyl sulfoxide at 20℃; for 0.5h;98.7%
1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

4-ethylbenzylaldehyde
4748-78-1

4-ethylbenzylaldehyde

(2R,5S)-2-(4-ethylphenyl)-3-methyl-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine
1042065-80-4

(2R,5S)-2-(4-ethylphenyl)-3-methyl-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Heating;98%
1,10-diisocyanatodecane
4538-39-0

1,10-diisocyanatodecane

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

N,N'-decamethylenebis[N''-(1-deoxy-D-glucitol-1-yl)-N''-methylurea]
1056030-07-9

N,N'-decamethylenebis[N''-(1-deoxy-D-glucitol-1-yl)-N''-methylurea]

Conditions
ConditionsYield
In 1,4-dioxane; water at 20℃; for 2h;98%
4-(((1S,2S)-2,3-dihydro-1-hydroxy-2-(1H-inden-2-yl)-1H-inden-2-yl)methyl)benzoic acid
1380445-03-3

4-(((1S,2S)-2,3-dihydro-1-hydroxy-2-(1H-inden-2-yl)-1H-inden-2-yl)methyl)benzoic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

(2R,3R,4R,5S)-6-(methylamino)hexane-1,2,3,4,5-pentanol 4-(((1S,2S)-1-hydroxy-2,3-dihydro-1H,1'H-[2,2-biinden]-2-yl)methyl)benzoic acid
1380445-04-4

(2R,3R,4R,5S)-6-(methylamino)hexane-1,2,3,4,5-pentanol 4-(((1S,2S)-1-hydroxy-2,3-dihydro-1H,1'H-[2,2-biinden]-2-yl)methyl)benzoic acid

Conditions
ConditionsYield
In methanol at 55℃;98%
In water
gadolinium(III) oxide

gadolinium(III) oxide

diethylenetriaminopentaacetic acid
67-43-6

diethylenetriaminopentaacetic acid

1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

gadopentate dimeglumine

gadopentate dimeglumine

Conditions
ConditionsYield
Stage #1: diethylenetriaminopentaacetic acid; 1-deoxy-1-(methylamino)-D-glucitol In water for 0.0333333h; Sonication; Green chemistry;
Stage #2: gadolinium(III) oxide In water for 0.3h; Sonication; Green chemistry;
98%
1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

aprepitant
170729-80-3

aprepitant

Fosaprepitant dimeglumine

Fosaprepitant dimeglumine

Conditions
ConditionsYield
Stage #1: aprepitant With dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate; sodium hexamethyldisilazane In tetrahydrofuran at -3℃; for 2h;
Stage #2: 1-deoxy-1-(methylamino)-D-glucitol With palladium 10% on activated carbon; hydrogen In methanol; water for 4h;
98%
1-deoxy-1-(methylamino)-D-glucitol
6284-40-8

1-deoxy-1-(methylamino)-D-glucitol

fosaprepitant

fosaprepitant

fosaprepitant dimeglumine

fosaprepitant dimeglumine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol; water for 4h;98%

6284-40-8Upstream product

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