Chemistry Letters p. 1951 - 1952 (1982)
Update date:2022-07-29
Topics:
Masuyama, Yoshiro
Usukura, Masa-aki
Kurusu, Yasuhiko
The reaction of 1,2-diols with dimethyl sulfoxide-catalytic molybdenum peroxide in refluxing toluene generally resulted in monoprotection of diols to give 2-methylthiomethoxy-1-ols (Course A).Exceptionally, a) cis-1,2-cyclooctanediol and benzopinacol, and b) 1,2-cyclododecanediol caused C-C bond cleavage (Course B) and monooxidation (Course C), respectively as Scheme 1.
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Doi:10.1016/0008-6215(83)88280-9
(1983)Doi:10.1021/ol061906y
(2006)Doi:10.1039/b501942g
(2005)Doi:10.1016/j.tet.2005.02.070
(2005)Doi:10.1039/jr9380000660
(1938)Doi:10.1002/ardp.19422801003
(1942)
